Analysis of water samples for the campaign 1919-1920

(1)

~.ALYSIS

OF

./4

TER S.8M!>LES FOR THE

ClAM.P

IGlif 1919

- 1920

LOVELL

FACTORY

Copieo to:

THE GREAT

WESTERN SUGAR

COMPANY

General Supt.

Gonera.l

Chemist.

~

Asst.

Genl. Supt.

f\.sst.

Chief

.Engineer.

Superintendent.

Traveling

Chemist.

Laboratoryo

(2)

T ! •

Page

/

LovellCity

wate

r ••••••.••..•••••••••••••••••••••••••••••••••••••••••• l

~

River

r:a

ter

from Shoshone

Rive

r •••••••••••••••••••••••••••••••••••••••

2 Lovell

City

wate

r,

boiled and

cooled. (Drinking

vm..te

r) ••.••••••• , •••• ,3

Legpipe

vm.tc

r

fro?11

the condensers

of Pan

"

A"

(

m1ite)

••••••••••••••••••

4 Legpipe

water from

condenser

of Pan

"B"

(

Reme

lt)

. . . 5

Le

gp

ipe

water

from

the

Evaporator

condenser

•••••.•••••••••••••••••••••

6 \

(

~

Battery Supply

\'later

(sin

g

l

e

system)

••

,

•••••••••••••••••••••••••••••••

7

1 \7a

ter

used for washing Hot

Pres

s

es

••••••••••••••••••••••••••••••••••••

8 ¢

\Va

ter

f

ro

m Bo

iler

r..,eed

Tank

•..•.•••••••.•••••••...•••••••••••..•...•.•

9 Condensed

water

from

the

Ev

aporc:,.

tor

d

ri

p

s •••••••••••••••••••••••••••• 10

:5-

Condensed

water

f

ro

,

m

Pan

coils

••••••••••••••••••••••••••••••••••••••• 11

Condense

d wa

t

er from Genera

l

Drips

••••••••••••••••••••..•••••••••••••

12

(3)

Form44i'-6m- l'-20-Paclt 100

WATER ANALYSIS

THE GREAT WESTERN SUGAR COMPANY

_ _ _

_

L

~QJ_E_

_L

~

I

-,_ ~

_.

_-

_Factory

L

ove

ll Cit

y water

.

~-~-JJ.me

10

~

_________

J

92 Q__,_

Kind of Water:

DescriptiGn of Sample:

_{Average samp}

_l

_{e for the}

_C

_ampa

_i

_gn.

Source of Water:

Ci

t

y

Main

,

dire

ct

from

ci

ty supp

l

y

t

ank

o

Sample ta..~en from tap in

Off

ic

e bu

il

ding

.

N

ot

e:

Cit

y wa

t

er was n

o

t used in an:y fa

ct

ory operations

,

ex

c

ep

t

as an emergen

c

y

supp

l

y t

o t

he B

oil

ers

.

ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid S04 Carbonic Acid C03

Organic and Volatile (by difference) TOT AL SOLIDS COPIES TO

General Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory

Part, Per I00,000

l

.

96 .1

4

6 .

82 l

o72

24

0

2

7

2 .

23

00 .

2

0

1

3 .

00

1

00 .

34

5 .

7

9 l

06 ol3

I.

HYPOTHETICAL Silica Si02

Sodium Chloride NaCl Sodium Sulphate Na2S04

Sodium Carbonate Na2C03

Magnesium Chloride MgCl

Magnesium Sulphate MgS04 Magnesium Carbonate MgC03

Calci1HD Chloride CaC12

Calcium Sulphate CaS04

Calcium Carbonate CaC08

Ferrous Carbonate FeC0₃

Organic and Volatile (by difference)

TOT AL SOLIDS COM31NATIONS Parr, Per I 00.000

1

7.

03 .

2

9

100

0

34 5.'79

1 06013

cJ

~_<ftr_.

1~y!

L

1' Chief Chemut.

(4)

'

Form441h,6m-11020--t.?ada IOO /

_ _

_,,L

_

QVELL

_

WATER ANALYSIS

_Factory

.IU!J.o

_

10 _,

Kind of Water:

River Water from Shoshone River.

DescriptiQn of Sample:

_{Average sample for the}

_Campaign.

Source of Water:

_Shoshone

_River

_{{ factory intake).}

_{Main source}

_of

_{supply for}

_all

factory

operations.

Sample

taken

from Main Supply pump.

ANALYSIS Silica SiO• Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine CI Sulphuric Acid

so.

Carbonic Acid

co.

Organic aad Volatile (by difference) TOT AL SOLIDS COPIES TO Parla Per I 00,000

6.64 .00

6.80

2.67

10.45

1.57

31.03

9.78

69.02

1.06

70.00

HYPOTHETICAL COMBINATIONS Silica Si02

Sodium Chloride NaCl

Sodium Sulphate Na2S04

Magnesium Chloride MgCI

Magnesium Sulphate MgS04

Magnesium Carbonate MgC03

Calcium Chloride CaCl2

Ferrous Carbonate FeC03

Organic and Volatile (by difference) TOT AL SOL.IDS

_

J9'i!_

_

Parts Per I 00,000

6.64

2.59

29.12

13.22

1.12

16.16 .17

69.02

1.06 70008

General Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory

:Z..

d

11 I

f,

_(!{r,.

~

. ~

-' Chief Chemist.

(5)

I

r

Form 4411-'-6m-lt.20-.!Pada 100

WATER ANALYSIS

_ _ _

__.,,,_,QU---cV11---.1E:...-.LL.,_L-

_ ___

_

Factory

_____

J:u.na

.10,

1.920 _

192 _ _

Kind of Water: Descripticm of Sample:

Source of Water:

l'Tote

:

Lovell Cit

y water,

boiled and

cooled. ( Dri:n1

ri~

water)

Average

samp

le

for

t

he

Cam

pa

i

gn.

.

City

wa

ter

fr

o

m

Cit

y

Supply

tank.

boiled and

coole

d.

Water was n

ot

used

i

n

factory operations. Used for dri:nlring

purposes

,

and for cooli

ng

pump

bea.ringso

---ANALYSIS Silica SiO, lroa Fe

Ctwcium

Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid S04 Carbonic Acid C03

Organic and Volatile (by difference) TOT AL SOLIDS

COPIES TO General Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory Part, Per I 00,()00

2.38 .10

7.13

1.85 25034

2o-23

54.15

12.69 105e87

6072

112059

Sodium Chloride NaCl Sodium Sulphate Na9SO,

Sodium Carbo11Bte Na2C03 Magnesium Chloride MgCl Magnesium Sulphate MgS04

Magnesium C~bonate MgC03

Calcium Sulphate CaS04 Calcium Carbonate CaC03 F .,rrous Carbonate FeC03

Organic and Volatile (by difference) TOT AL SOLIDS Parts Per 100,000

2.38

3.68 73078

5.34 2o67

17081

.21

105.87

6.72

112.59

(6)

Form 443...- 6m- f-20-l.?ada IOO )

WATER ANALYSIS

_ _ _

_

L~Q

V E L

I,

_{_}

_Factory

_{_}

_{.Jun~ lit,}

_{__}

Kind of Water:

Legpipe water from the

condensers

of

Pan

"A"

(

\Thi

te

) •

Average

sample for the

Campaign.

_

192~

-Source of Water:

Shoshone River water from the Main iater Supply tank, and

condensed

vapors

from

White

Pan

Liquors.

ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulphuric Acid

so.

Carbonic Acid

co,

COPIES TO General Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory Parlt Per I 00,000

2.19 .11

6.62

2.44

9.93

1.49

29.78

9.13

61.69

2.19

63.88

HYPOTHETICAL COMBINATIONS Parts Per I 00,000 Silica Si02

2.19

2.46 27067

Magnesium Sulphate MgSO,

12.08

2.03

15.03 .23

61.69

2.19

TOT AL SOLIDS

_63.88

·~_f!Y(_,___

L ,

d

~~

I

fl

(7)

Fo,m 448-'-6m- l'-20-lpads 100 J

LOVELL

Kiod of Water: Description of Sample:

WATER ANALYSIS

_ _ _ _

Factory

:Legpipa

wa

ter

from

con

denser

of Pan

11

B"

l

_Remelt}.

Average

sample

for

t

he

Campaign.

JU.ne

10,

_{. __}

_{192_0}

_{_}

Source of Water:

_Shoshone

_R

_iver

_{water from the Ma.in water SUpply tanl~.}

_{gondensed va}

_p

_ors

from

Remelt

Pan

Liquors.

ANALYSIS Silica SiO, lroa Fe Cailcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid

so.

Carbonic Acid

co.

COPIES TO General Supt. General Chemist A9St. Genl. Supt.

~ t . Chief Engineer Superintendent Traveling Chemist Laboratory Part, p.,. I 00,000

81178

.o9

5.61

2.59 9.oa

1.45

30.14

6.69

64.43 l.60

66.03

HYPOTHETICAL COMBINATIONS Part, Per I 00,000 Silica SiO,

_8.78

2.39

25.14

Sodium Carb0D11te Na,C03

12.a2

Magnesium Clll'bonate MgC03

4.12

10.99 .19

64.43

Organic and Volatile ( by difference)

1,60

(8)

, I Form 44a-6m-1~20-Pada IOO

WATER ANALYSIS

L O V

E

L L

_ _ _ ______

factory

Kind of Water: DescriptiGn of Sample:

Legpipe

water from the Evaporator

condenenr.

A

verage

sample

for the

Campai

gn

.

t

/'

t}'wle

_

10,

_{_}

₁₉₂

_{_0}

_{_}

Source of Water:

_{Shoshone River water from}

_t

_{he Main}

_{water supply tanlr.}

_Condensed

_vapors

from the

liquor

s

of the fifth effect of the Evaporators.

ANALYSIS Silica Si02 lroa Fe C~um Ca Magnesium Mg Sodium Na Chlorine CI Sulphuric Acid

so.

Carbonic Acid C03

TOT AL SOLIDS COPIES TO

General Supt. General Chemist Aost. Genl. Supt.

Asst. Chief Engineer Superintendent Traveling Chemist Laboratory Part, P« I 00,000

3.85 .15

8.41

2.67

9.72

1.45

30.35

11.84 68044

2o97

71.41

HYPOTHETICAL COMBINATIONS

Parts Per W0,000

Silica Si0,

_3.85

2.39

27.11

Sodium Carbo!lllte Na2C00

13.22

Magnesium Cifbonate MgC03

2o08

19048

.31

68044

2.97

TOT AL SOLIDS

_71.41

(9)

WATER ANALYSIS

LOVE.1.iL

_Factory

_{____}

_June

_{_}

₁₀

_•

Kind of Water:

_{Battery Supply ater ( sin5:le s~rstem ·).}

Descriptie>n of Sample:

_{Average Sample for the Ce.mpaignc,}

Source of Water:

\7ater from the Evaporator condenser,legpipe, overflow from the

.Pross ·;rash Tc.nJ.:, and the overflow from the legpipe seal tank

.

ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulphuric Acid

so.

Carbonic Acid

co.

Organic and Volatile (by difference) TOT AL SOLIDS COPIES TO Parts Per I 00,000

l

o

84 .05

a

.

73

2 .

57 a.74

1 .

39

29 .

20

11.45

63 .

97

2 o

96

66

0

93

HYPOTHETICAL COMBINATIONS Silica _SiO•

Organic and Volatile lby difference) TOT AL SOLIDS

_

I 92_Q__

_

Parts Per 100,000

1.84

2 .

20

24

0

21

12.72

3

0

80 19.0l

o

lO

63

0

97

2 .

96

66 .

93

Genl!ral .Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory

7. (}fy

.

~ 1 _ ~

· -

~= - -- " _

(10)

, I

Form44ll-6m- 11_-20_-_Pado₁₀₀

r •

WATER ANALYSIS

L

O

V 1LL

_

_li

_ __

_

_{_}

_Factory

_{_}

_J3me

₁₀

_,

_{_}

_19.20

_{_}

_~

Kind of Water:

i'later

used

for

washiro,S

H

o

t

Presseso

DescriptiQn of Sample:

Average Sample

for

the Cam:paigno

Source of Water:

Dl'"ips

frocn

all

ro...:heaters, first effect of the Evaporators,

and

high...green,

and

high-wash

blo·.v..ru.p ta.nlcs

.

Over>-flovr

from

the

Boiler

Feed

Tank

o

.AJ.so possible

to

s011d drips

from the

second a..~d third effects

of

the Evaporators

and

GranuJ.ator Traps

.

ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium

Na

Chlorine Cl

Sulphuric Acid

so.

Carbonic Acid C03

Genffal Supt.

General Chemist Asst. Genl. Supt. Asst. Chief Engineer

Superintendent Traveling Chemist Laboratory Part, Per 100,000

.

27 .

06 .

46 .

12 r,72

0

84 lo

57 .

30

4 .

34

7 ~

86

12

0

20

HYPOTHETICAL COM8INATIONS

Paris Per 100,000

Silica Si02

027

1

0

38

056

0

59 l

o

02 o

4D

0

12

4 o

34

Organic and Volatile (by difference}

7

0

86

(11)

Form443-' >m-t•-io--yPado 100

- - -

-L

~

o=--y_

E

L L

Kind of Water: DescriptiGn of Sample:

WATER ANALYSIS

Factory

Water

from

Boiler Feed Tank.

Average sample for

the Campaign.

June

10,

___

192 _

0 _

Source of Water:

Drips

from

the

second,

third, fourth

and

fifth

effects

of the

~vaporators,

Main steam

line trap, and drips from the Granulator trap. Po~sible to

send

drips

from

Pan "A" and

Pan

"B" Coils,

and

General Drips, to

Boiler Feed

Tank; otherwise these are

pumped direct

to

Boilers.

ANALYSIS Silica SiO, Iron Fe Calcium Ca Magnesium ·Mg Sodium Na Chlorine Cl

Sulphuric Acid

so,

Carbonic Acid C03

Gen~al Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Su~rintendent Traveling Chemist Laboratory Part. Per 100,000

1.35 .06

1.05 .26

3.60 .84

4.43

3.00

15.09

1.10

16.19

HYPOTHETICAL COMBINATIONS Parts Per I 00,000 Silica Si02

1.35

1.38

Sodium Sulphate Na,S04

6.55

2.17

Magnesium Sulphate MgSO,

Magn.esium Carbonate MgC03

.90

2.62 .12

15.09

Organic and Volatile tby difference)

1.10

TOT AL SOLIDS

_16.19

/I

l

(12)

Fona44iJ 'm-1°-21>-iPacLi 100 ( I \

WATER

ANALYSIS

- - - - '

L=---0

--=-V

E

L

__

L

Factory

_ J'.LlllC

_

lQ

I

___

192 _

0 _

Kind of Water:

Condensed

water from

the

Evaporator drips

Description of Sample:

Average 3a.tnple fpr

the Ca.tnpaign.

Source of Water:

Condensed

water from

the

drips of the first, second,

third, fourth

and fifth

effects of the

Evaporators.

ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid 504 Carbonic Acid C03

TOT AL SOLIDS

COPIES TO Genrral Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer

Superintendent Traveling Chemist Laboratory Parts Per I 00,000

.51

.06

.21

.o5

.01

.27

.29

.18

1.64

1.45

3.09

I~-HYPOTHETICAL C0M81NATI0NS Silica Si08

Magnesium Chloride MgCl Magnesium Sulphate MgS04

Organic and Volatile {by difference)

TOT AL SOLIDS Parts Per I 00,000

.51

ol8

.20

.02

.41

.20

.12

1.64

1.45 d ~/"

_{• (J}

_a

_{_}

_{r ._ _}

1 ~

_{_ __ _}

_-

t,

C 'ef ChemiSl,

(13)

Form 4411-, 6m-1~2o-1 Pad. 100 (

WATER ANALYSIS

LOVELL

_~

_Factory

_{----~- _}

_June

₁₀

_,

_{_}

_{l92Q__}

Kind of Water:

_Condensed

_{water from}

_J?a.n

_coils.

_{Average sample for}

_{the Campaign.}

On

removal of

coils

after campaign, one was found to be fu.1.1 of sugar.

This accounts for the high orga:nic figu.re in the analysis.

Source of Water:

_Condensed

_{water from the}

_coils

_{of Pan}

_{"A" (}

_White

₎

_and

_Pall

_"B"

_(Remelt)

pumped direct to

the

boilers, also possible

to

send

condensed

wa.ter from the General

drips, which includes the

condensed water from all .Pan Rtorage

tank coils,

and second

and

third Carbonation

tank

coils.

Also possible

to

send

condenoed

waeer from

Pan

coils

to

Boiler Feed tank.

ANALYSIS Silica Si02 lroa Fe Cllllcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid

so.

Carbonic Acid C03

General Supt. General Chemist A!st. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemiot Laboratory Parts Per I 00,000

062 .10

1.39 .37

2.95 .20

4.4.0 4o03

14.06

89.17 //.

HYPOTHETICAL COMHINATIONS Silica Si02

Sodium Chloride NaCl Sodium Sulphate Na2S04

Magnesium Chloride MgCI Magnesium Sulphate MgS04

Magnesium c..,honate MgC03

Calcium Chloride CaCl2 Calcium Sulphate CaS04

Organic and Volatile {by difference) TOT AL SOLIDS Part, Per I 00,000

14.06

89

9

17 _

n.

arr~

1 _ ~ ,

·

11 V

Chief Chemist.

(14)

Form 443 m- t-2o-J,'aclo I 00 f

l

WATER ANALYSIS

L O

V

E

L

----

== _

_

Factory

June

10 • 1-920

_ _ _

192 __

Kind of Water:

Condensed

water from

General

Drips.

Average

sample

for

the

Ca.m1:>aign.

Source of Water:

Condensed

water

from all

J?an

Storage

tank coils,

first, second and

third Carbonation tank coils,

and possible

to

send

condensation from

Ma.in

Steam

line trap•

pumped

diroct to the

Boilers.

ANALYSIS Silica Si02 lroa Fe c.c,ium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid

so.

Carbonic Acid C03

Organic a11d Volatile (by difference) TOTAL -50L1DS

COPIES TO General Supt. General Chemist

A:!St, Genl. Supt. ASl!t. Chief Engineer Superintendent Traveling Chemist Laboratory Parts Per I 00,000

.47

.12

054 .20

.55

.39

1.32

1.01

Sodium Sulphate Na8SO,

Sodium Carbonate Na,C03

Magnesium C.hloride MgCl

Organic and Volatile thy difference) TOT AL SOLIDS

)~.

Part, Per 100,000

086 .10

lo35

025 a.as

(15)

I

Form 448--, 111- 11.2o-l•ada 100 L I

WATER ANALYSIS

LO

VE

_L_-.L

_ _

Factory

Water

in

Boilerso

J\UJ,e

lO,

_

192__0_

Kind of Water:

_{Average sample for the Campaign.}

Source of Water:

_{Water from the Boiler Feed tank, condensed water from the General drips,}

a.nd

condanaedwater from

ai.l.

Rm

coils.

Noto:

No

Soda

Ash added to the Boilers d:u.ring Campaign.

ANALYSIS Silica Si02 lroa Fe C._!cium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulphuric Acid

so.

Carbonic Acid

co

.

General Supt. General Chemist A951. Genl. Supt. A9't. Chief Engineer Superintendent Traveling Chemiot Laboratory Parta Per I 00,000

4.15 .95

8071

lo22

2lo00

2o28

11.67 36029

87.07

57.12

HYPOTHETICAL Silica SiO,

Sodium Sulphate Na,S04

Sodium Carbollllte Na2C03

Magnesium C,.:bonate MgC03

Oraanic and Volatile lby difference)

TOT AL SOLIDS COMBINATIONS Puta Per I 00,000

4

0

15 3o76

17.26 33095

21075

1.97

87.07

57.12 _ _ _ _ _ _ _

l44ol9

/J.

d

·- <Jry_,__

- "'~- -

~

-

-' ] ~ J _ A

Chief Chemist.