Analysis of water samples for the campaign 1920-21 Eaton factory

(1)

6£ 'L CK-EM'S i.;frit;E

G. W.

s.

CO.

THE GREAT WESTERN SUGAR COMPANY

EA TON FACTORY

ANALYSIS OF WATER SAMPLES FOR THE CAMPAIGN 1920-21

Copies to:

General Superintendent

General

Chemist/.--Assistant Chief

EnginMr

Superintendent

Traveling Chemist

Laboratory

(2)

(3)

EA.TON

_Factory

Kind of Water:

City

tiater

DescriptiGn of Sample:

A.ve;rage tor

the

eampa1gn.

Source of Water:

City Mains. 1211s water is pumped

fro1n

ile north.

west

ot

the

Faotoey.

ANALYSIS Silica SiO. Iron Fe c.,:ium Ca Magnesium Mg Sodium Na Chlorine CI Sulphuric Acid 504

Carbonic Acid

co.

Organic and Volatile (by difference} TOT AL SOLIDS COPIES TO

General Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory Paris Per I 00.000

3.54 .27

10.43

2.18 '7.39

2.09

22.72

14.95

63.67 3.7~

67.30 --~

C8?Jll>&ign

_

1920-2!

__ _ .

1921

.

lle, 86 feet deop, located

about one-halt

HYPOTHETICAL COMBINATIONS

Parts Per I OQ,000

Silica SiO•

3.54

Sodium Chloride NaCl

3.45

Sodium Sulphate Na2S04

18.62

Sodium Carbonate Na2C03

Magnesium Chloride MgCl

Magnesium Sulphate MgS04

10.78

Magnesium Carbonate MgC03

Calci1HD Chloride CaCl2

Calcium Sulphate CaS04

2.17

Calcium Carbonate CaC03

24.45

Ferrous Carbonate FeC03

056

3.57

Organic and Volatile (by difference}

3.73

TOT AL SOLIDS

_6'7.30

(4)

THE GREAT WESTERN SUGAR COMPANY

Eaton

_{_ __}

_Factory

_{Camp11,ign 192 O._?l}

_{__}

_J

_92L

_{_}

Kind of Water:

Ditch Water.

Description of Sample:

A'Yerage Sample for the Campaign.

Source of Water:

Water ta.fen from

Boye•

s Seepage

ditch about one-fourth

mile :East of

factory.

ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid S04 Carbonic Acid C03

Organic aiad Volatile (by difference)

TOT AL SOLIDS

COPIES TO Genffal Supt.

General Chemist

-Asst. Genl. Supt.

Asst. Chief Engineer

Superintendent Traveling Chemist Laboratory Par11 p.,.. 100,000

3.10 .20

9.82

2.87

6.90

2.37

28.48

11.19

64.93

5.17

70.10 Page 2

HYPOTHETICAL COMBINATIONS Pull Per 100,000 Silica Si02

3.10 _3.91

Sodium Sulphate N ...

so

4

16.55

Magnesium Sulphate MgSO._

14.19

Calciooi Chloride CaCl2

Calcium Sulphate CaSO~

8.46

18.31

Fenous Carbonate FeC03

041

64.93

Organic and Volatile tby difference)

5.17

(5)

_

_ _ _ _

EA

_

TO.N

_ _ _ _ _ _

Factory

_--~-

_{O!UDPaign 1920-21}

_{_}

_.

₁₉₂

_l

Kind of Water: Descriptign of Sample: Source of Water: Silica Iron Calcium Magnesium Sodium Chlorine Sulphuric Acid Carbonic Acid

Pure

.Battery SUpply Water.

Average Sample for the Campaign.

Overtl.ow

rrom

Press

P

ash and Seal Ta.llk:s.

High

"

Organic " percentage due

tt presence of sugar

and

:non-sugars. This was

• not

uaed at intervals of several

daya

and at times boos.too quite stagnant.

On several occasions the water

was so

heavy in sugar that

it

was nece

· ssary to

empty

the

tank.

ANALYSIS _{HYPOTHETICAL COMBINATIONS}

Par11 Pet I 00,000 Part, Per IOQ,000

SiO,

_2.48

Silica Si02

2.48

Fe

_.04

2.18

Ca

_6.55

Sodium Sulphate Na2SO,

12.63

Mg

1.ae

Na

_4.95

_{Magnesium Chloride} _MgCI

CJ

_1.32

_{Magnesium Sulphate}

_Mgso.

7.66 so.

14.65

1.14 co

.

10.65

CalcitHD Chloride CaCl2

Calcium Carbonate CaC0₈

16.35

Ferrous Carbonate FeC0₃

.oe

42.52

Organic and Volatile (by difference) TOT AL SOLIDS

10.68

53.20

Oraanic and Volatile {by difference)

11).68

TOT AL SOLIDS

5.'5.20

COPIES TO General Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory

(6)

WATER ANALYSIS

-

- -

--=EATQJ

_

Factory

0&Jll)&lgn 1920-21

Kind of Water: Description of Sample: Source of Water: Silica Iron Calcium Magnesium Sodium Chlorine Sulphuric Acid Carbonic Acid

Impure

Battery supply

1,.,Ja

ter.

Average Sample

tor the Campaign.

Vat

er fen

White

Pan

(

A)

Condenser

BrownPan

(JS)

Condenser

Brown Pan (

O) Oondenaer

:Evaporator

Condenser

and

overtlow

from

Oryatallisere.

Part• Per I 00,000

Si02

3.24

Silica Si02

Fe

_.04

Ca

_10.29

Sodium Sulphate Na,SO,

Mg

2o83

Na

,.2,

_Magnesium_Chloride _MgCI Cl

_1.,0

_{Magnesium Sulphate} _MgS0

4

so.

23.01 co.

14.85

Calcium Chloride CaCl2

,2

..

12

Organic and Volatile (by difference} TOT AL SOLIDS

5.'8

,,.so

Organic and Volatile (by TOT AL SOLIDS difference) COPIES TO

Genrral Supt. General Chemist Asst. Genl. Supt. Ass!. Chief Engineer Superintendent Traveling Chemist Laboratory

'_

J9D,.

__

Part, Per I 00,000

3.24 2.'4

1,.12

13.99

1.35 24.'10

.oe

,2.12

s.,e

,1.ao

(7)

R 'l'OR

-

- -

- - - -

Factory

Campaign 1920•21

Kind of Water:

ater

fro

:hit

(

A

)

Condenser.

_{Average Sa.mpl}

tor

_the

_Oampa.1gn.

Source of Water:

_Ditch

_:

_a.ter

_nd

_cond0naat1on

_from

_{ih1to Pan.}

ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid

so.

Carbonic Acid

co,

Organic and Volatile (by difference) TOT AL SOLIDS COPIES TO Parl, Per 100,000

3.78 .06

8.46

2.11

1.11 1.a1

23.25 12.ao

60.04 &.oo

66.04

HYPOTHETICAL COMBINATIONS Silica Si02

Magnesium Chloride MgCl Magnesium Sulphate MgS04

Ferrous Carbonate FeCOa

Organic and Volatile lby difference) TOT AL SOLIDS

_

192_!

_

Pari. Per 100,000

3.78

2.98

18.35

13.68 .10

:zi.13

.1.2

60.04 &.oo

66.04

General Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent

Traveling Chemist

Laboratory

(8)

Kind of Water: Description of Sample: Source of Water: Silica Iron Calcium Magnesium Sodium Chlorine Sulphuric Acid Carbonic Acid

WATER ANALYSIS

.Factory

Water

from Brown

Pan

(

B)

Condenser.

Average

Sample tor

the

Campaign.

Camp~1gn 1920-21

Ditoh ater and condensa.t1on fro,n

Brown

Pan (

:S

).

Paris Ptt I00,000

Si02

i.78

Silica Si0₂

Fe

.06

Ca

9.08

Mg

_2.85

_{Sodium Carbonate} _Na

0C03

Na

_7.00

_{Magnesium Chloride} _MgCI

Cl

1.67

4

so.

23.95 co

.

_13.43

CalcitHD Chloride CaCl2

61.82

TOT AL SOLIDS

6.48

68.30

•

TOT AL SOLIDS COPIES TO

_

1921__

__

Paris Per 100.000

3.78

2.75

18.28

14.09 .50

22.30 .12

61.82

6.48

68.30

Genrral Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer

Sup,,rintendent

Traveling Chemist Laboratory

Page 6

(9)

:ATON

- - - -

_

Factory

Campaign 1920-21

Kind of Water: 1

_{ater from Brown Pan}

₍

_{C) Condonso!".}

DescriptiQn of Sample:

_{Avera.go Samplo for the}

_Oamapign.

Source of Water:

_{Ditch water and oondensat1on from Brown}

_.Pan

₍

_O

_).

ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulphuric Acid

so.

Carbonic Acid

co

.

Organic and Volatile (by difference) TOT AL SOLIDS COPIES TO

General Supt. General Chemist Asst. Genl. Supt. AMt. Chief Engineer Superintendent Traveling Chemist Laboratory Parr. Per 100.000

3.30 .11

9.59

2

• .,s

6.71 l.89

22.96

14.14 -61.48

4.98

66.46 Page 7

HYPOTHETICAL COMBINATIONS Silica Si02

Sodium Chloride NaCl Sodium Sulphate Na2S04

Magnesium Chloride MgCI Magnesium Sulphate MgS04

Calcium Chloride CaCI. Calcium Sulphate CaS04

Ferrous Carbonate FeCO,

Organic and Volatile thy difference) TOTAL SOLIDS

_

192!_

_

Parts Per I 00.000

3.3Q

3.12

16.92

13.75 .78

23.38 .23

61.48

4.98

66.46

(10)

WATER ANALYSIS

______

Factory

C8IIJPl'!lg'l1

l,920-21

_

J

92.l._

_

Kind of Water:

ater from Evaporator Condenser.

ATarage Sample :tor tl1e Oanrpalgn.

Source of Water:

_{Ditch ater and condensation trom the 5th Effect of the .EVaporatora.}

ANALYSIS Silica SiO, Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulphuric Acid

so.

Carbonic Acid C03

Organic and Volatile (by difference) TOT AL SOLIDS COPIES TO

Gen~ral Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendttnt Traveling Chemist Laboratory HYPOTHETICAL COMBINATIONS Partt Pe. f00,000

3.88

Silica SiO•

.13

10.73

Sodium Sulphate Na,S04

2.eo

6 a69

1.91

23.42

15.79

65.43 ,.21

Organic and Volatile (by difference)

69.64

TOT AL SOLIDS

Page

8

Partt Per I 00.000

3.88

3.

1

_.5

16.83

14.24 .96

26.10 .27

65.43 4 .. 21

69.64

(11)

Kind of Water: DescriptiGn of Sample: Source of Water: Silica Iron Calcium Magnesium Sodium Chlorine Sulphuric Acid Carbonic Acid

_

Factory

Prese

ash

Water.

Averagoe

Sample

tor the

Campaign.

oazrmaign 1920-~l

__

192.i_

__

Water :from

all

High

and

Low

EXhaust Traps;

everflow

from

.Boiler Peed

Tank;

Water from

aoils of Brow

Pans

(

B

&

C ) ,also

from Wh1

te

Pan (

A ) coils

part

of

the

Campaign.

Water from

all Steam

Chests

of the EVaporatora

and

drips

£rom all

Heate~s.

Parts Per !00,()()0 Part, Per 100,000

Si02

.74

Silica _Si0₂

~·14

Fe

.03

.36

Ca

.'18

_Sodium_Sulphate _Na

2SO,

2.10

Mg

.22

_{Sodium Carbonate} _Na

2C03

Na

.e2

_Magnesium_Chloride _MgCI

CI

_.21

4

~es

so.

3.17

C03

.52

Calcium Chloride CaCI₂

1.54 .82

.o,

,.49

G.49

2.70 e.19

Organic and Volatile lby difference)

2.70

TOT AL SOLIDS

9.19

COPIES TO Gen~ral Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist

Laboratory

Page 9

4 ~

(12)

WATER ANALYSIS

- - - -

-

~EA.,,.'D-

- - -

__

Factory

Campaign 1920-?l

___

1921

__

Kind of Water: Description of Sample: Source of Water: Silica Iron Calcium Magnesium Sodium Chlorine

ater from Boilers.

Average SIPDJ)le

fer

the

Osmpaigf'1•

Water trom Boiler Feed

Ta:llk.

Condensation from r.hite Pan Coils.

ANALYSIS Parts Per 100,000 SiO!

_1.84

Silica Fe

_.15

_{Sodium Chloride} Ca

_2.69

Sodium Sulphate Mg

_.23

Sodium Carbonate Na

_47.14

_M_{agnesium Chlorid}_e Cl

_5.58

_{Magnesium Sulphate}

HYPOTHETICAL COMBINATIONS

SiO, NaCl Na,S04 Na2C03 MgCI MgS04

Sulphuric Acid S04

59.76

Magnesium Carbonate MgC0₃

Carbonic Acid

co

a

Organic and Volatile (by difference} TOT AL SOLIDS COPIES TO

General Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory

24.20

CalcilHII Chloride CaCl2

Calcium Sulphate Ca.504

141.59

33.65

Organic and Volatile {by difference}

175.24

TOT AL SOLIDS

Pago 10

Parts Per l 00.006

1.84

9.20

88.36

34.34 .so

6.72 .31

141.59

33.65

175.24

Chief Ch

(13)

e,;;;;.--EATON

_{_}

_Factory

_Camne,1gn

_{_}

_l920-2i

_~

_{192_1}

_{_}

Kind of Water: Descriptign of Sample: Source of Water: Silica SiO, Iron Fe Calcium Ca Magnesium Mg Sndium Na Chlorine CI

Sulphuric Acid

so.

Carbonic Acid

co

.

7 ater from Boiler Feed Tank.

Average Sample for

the

Campaign.

Includes

water from Steam Chests of all the

Evaporators.

Condensations from coils of White (A} and Brown ( B) Pana.

City

and

Ditch

Waters

.

Parll Per 100,000

1.52

Silica SiO•

.06

l.80

Sndium Sulphate Na2S04

.fi2

Sndium Carbonate Na2C03

8.35 .10

e.e1

9.09

Calcium Chloride CaCI,

Calcium Sulphate CaS0₄

Calcium Carbonate CaC0₈

3>.95

2.91

33.86

COPIES TO Genl!ral Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory

Page

11

Part, Per 100,000

1.02

1.15

13.03

8.48

2.15

4.50 .12

30.95

2.91

33.86

(14)

WATER ANALYSIS

EAroN

_ _ _

F

actory

_ _

Camm!,1m_l920-2l

_ _

J91).J.

Kind of Water: Description of Sample: Source of Water: Silica SiO• Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid S04 Carbonic Acid C03

Water from r.'h.ite

Pan Coils

(Pig).

Avera.ea

Semple

for. the CcJnpaign.

Condensation from

White

Pan

Coils.

ANALYSIS

Parts p., 100,000

.84

Silica

.03

Sodium Chloride

1.58

Sodium Sulphate

a41

Sodium Carbonate

2.26

Magnesium Chloride

.35

Magnesium Sulphate HYPOTHETICAL COMBINATIONS Si02 NaCl Na,S04 Na,C03 MgCI MgS04

6.21

Magnesium Carbonate MgCO.

2.17

Calcium Sulphate

easo.

Calcium Carbonl!te CaC08

Fenous Carbonate FeC03

13.85 l.105

14.90

Organic and Volatile tby difference) TOT AL SOLIDS COPIES TO

Gen~ral Supt, General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist