Analysis of water samples saved during the potash campaign of 1919-20

(1)

0

Thi. UilliAl1

WE

STERN SUG

A

H COl'L? ;.,NY

LOUGMOl?:.'

?AC~O...'W

..tt.liALYSIS OF WA'.::ER SA!.lPLES SAVED 1 ... UNG

'l.'HE POrASH CAJl.~!.IuH OF 1919

-

20 Copies to:

General Supt.

-

General Chemist,

Asst, Chief Engineer.

Superintendent,

Traveling Chemist.

Laboratory.

(2)

y

\'later

from Boiler

Feed Tank

'7

Water used

1n

washing

Hot

Presses

Legpipe

Water

from

1st

Condenser

or

North Evaporators

Legpipe Water from 1st Condenser ot South Eva:porat.Olrs

(

Drips

from 1st 'Ef'feot Jwa.porators

)

Drips fron 2dn 'Effeot Evatx>rators

/

Drips from 3rd Efteot EvaporatOJta

\

Drips from 4th Effect Evaporators

1

3

4

5

6

7

8

(3)

WATER ANALYSIS

THE GREAT WESTERN SUGAR COMPANY

I.ongm.ont

. _

_

Factory

_{May 21}

_{192o}

Kind of Water:

Water ~rom Boiler

Feed Tank

Descriptien of Sample:

Average sample for the Potash Campaign

Source of Water:

_{Drips from steam chamber of 2nd effect evaporators, and occasionally city water}

ANALYSIS Silica Si01 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid

so.

Carbonic Acid

co

.

Ponasiwn

K

Organic and Volatile (by difference) TOT AL SOLIDS COPIES TO

General Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory Par11 Per I 00,000

026 .20

lol3

.17

004

1.03

5.38 e33

2e69

16 .

06

HYPOTHETICAL COM13INATIONS Sodium Carbonate Magnesium Chloride Magnesium Sulphate Magnesium Carbonate Calcium Chloride Calcium Sulphate Calcium Carbonate F enous Carbonate MgCI MgSO, CaCl2 CaC03 FeC03

Organic and Volatile (by difference) TOT AL SOLIDS

Para Per 100,000

11.23 4,.83

(4)

_

_ _

...,L.,..ongmmi ______

Factory

________

14VY1,

_

_ _ _

192

0

Kind of Water:

Wo

ter used

tor

Washing

Hot

Presses

DescriptiGn of Sample:

Average Sample for the Potash Campaign

Source of Water:

_{Drips from steam chambers of 3rd,}

_4th,

_&

_5th

_{ettect evaporators}

ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid S04

Carbonic Acid

co.

Potassium

X

Organic and Volatile {by difference) TOT AL SOLIDS COPIES TO

Genn-al Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Parts Per 100.000

.30

1131

3.ao

.15

3o07

4.82

19.30

1.45 9.3'1

42057

30.63

HYPOTHETICAL COMBINATIONS Silica Si02

otassiwn Chloride Kol

bnizQ:m.e

~@c

otassium Sulphate

_~so

Sodium Sulphate

o.sd\

Sodium Carbonate Na2C03

Magnesium Chloride MgCl Magnesium Sulphate MgS04

Magnesium Carbonate MgC03 Calcium Chloride CaC12

Calcium Sulphate CaS04

Calcium Carbonate CaC03

Ferrous Carbonate FeC03

Organic and Volatile lby difference) TOT AL SOLIDS

Parts Per I 00,000

074

(5)

WATER ANALYSIS

__ _ _

Factory

Kind of Water:

Legpipe water f'rom

1st

Condenser

of

North Evaporator

Description of Sample:

.Average Ssnple for the Potash

Ce11aign

Source of Water:

_{Vapor condensed in 1st condenser}

_or

_{north evaporator}

ANALYSIS Silica SiO, Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid S04 Carbonic Acid C03

Potassium

K

Genrral Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory Puts Per 100,000

lo26

.34

18057

11.51

14.94 2e87

107.92

7.53 lo70

166.64 20156

187020

Potassium Chloride

Sodium Chloride NaCl Sodium Sulphate Na2S04 Sodium Carbonate Na2C08

Magnesium Chloride MgCI Magnesium Sulphate MgS04

Magnesium Carbonate MgC03

CalcilHD Chloride CaCl2

Calcium Sulphate C'.aS04

Ferrous Carbonate FeC03

Organic and Volatile {by difference) TOT AL SOLIDS Parts Per I 00.()()t)

l,o26

3.2§

2.1 43049

56.96

46.85

11.94 .11

166.64 20~56

187020

Chief Chemi91.

(6)

Longmont

.

__

Factory

May

21,

Kind of Water:

Legpipe water trom ls t condenser

of

South Evaporator•

Average sample tor

the:'.

Potash

Campaign

Source of Water:

_{Vapor oondensed in}

_1st

_{condenser of south}

_evaporators

ANALYSIS HYPOTHETICAL COMBINATIONS

Silica SiO• Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulphuric Acid

so.

Carbonic Acid

co.

Potassium

K

General Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent

Parta Per I00,000

1.26 .20

18.38 llol6

14.43 2o87

106.91 6012

1.61

162.94 20116

183.10

Silica SiO, P°s~::!~d?hloride _NaCl

Sodi.m Sulphate Na,S04

Sodium Carbonate Na.C03

Magnesium Chloride MgCI

Magnesium Sulphate MgS04

Calcium Chloride

eac1.

Calcium Sulphate CaSO,

Organic and Volatile lby difference) TOT AL SOLIDS

192o

Puts Per 100,000

126 i:8i

41.75

55.23

49.04 9 86

.41

162094

20.i6

183.10

(7)

WATER ANALYSIS

Longmont

_ _

Factory

_{--- _ --}

_~

_-

_~

_{- - - - -}

₁₉₂

_{_0_}

Kind of Water:.

Drips f'rom :t?o.

l

Evaporators

Average tor

trampaign-

oomposi

te of' North

&:

South Evaporators

Source of Water:

Water that condensed in tubes of' 1st etf'eot north

&:

South Evaporators

ANALYSIS Silica SiO, Iron Fe Calcium Ca Magnesium Mg

Sodium

Na Chlorine Cl Sulphuric Acid

_so.

Carbonic Acid C03

Potassium

X

Organic aad Volatile (by difference) TOT AL SOLIDS COPIES TO

General Supt, General Chemist Asst,

Genl.

Supt.

Azst.

Chief Engineer

Superintendent Traveling Chemist Laboratory Parta Per 100,000

.40

020 lo51

032

002 .41

s.2a

~49

.,.97

11.16

HYPOTHETICAL COMBINATIONS Silica SiO,

~ : : - Chloride~

Po.tass

1 imn

SulphateNK_so

4

Soclium Su phate a2

BO,

Sodium Carbonate Na,C03

Magnesium Chloride MgCI

Magnesium Sulphate MgS04

Calci1HD Chloride CaCI.

Oriianic and Volatile (by difference) TOT AL SOLIDS Parts Per I 00,000

~40

c,86

lo58

4o7Z

,

9.60 lo56

11.16

Chief Chemist.

(8)

Longmont

Factory

_ --~~-- _

1M~

.21,

_____

192_0

_

Kind of Water:

Drips trom

.2nd

ef'f'ect evaporators.

Average

San.ple f'or Potash

Cam:rsiign ...

Composite of North

&

South

evaporators

Source of Water:

_{Water that condensed}

_in

_tubes

_of

_{2nd effect North&: South evaporatoes}

ANALYSIS Silica Si01 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid S04

Carbonic Acid

co.

Potassium

X

Organic aad Volatile (by difference) TOT AL SOLIDS COPIES TO

General Supt. General Chemist Asst. Genl. Supt.

Aut. Chief

Engineer

Superintendent Pam P .. 100,000

032

020 lo72

.36

io6

1.13 7~28

82

3.36

15.25

6.95

22.20 P~~Chloride

P0tasaumSUlpbate

am

Sodium Sulphate Na2S04 Sodium Carbonate Na1C03

Magnesium Chloride MgCI Magnesium Sulphate MgS04

Calcium Chloride CaCl2 Calcium Sulphate CaS04 Calcium Carbonate CaC03 Ferrous Carbonate FeC03

·Organic and Volatile {by difference) TOT AL SOLIDS Porta Per I 00,000

.32

2ta38

4o70

.1a

1.78 4,o,46

1.02 .41

15.25 6095

224'20

(9)

WATER ANALYSIS

_ _ _

___...Lo

.... J:16U10nt__

_ _

_.

_Factory

_{___}

₁₉₂

_{_}

₀

_{_}

Kind of Water:

_{Drips trom 3rd etteat enporators}

Descripti<>n of Sample:

.Average sample

:foe

the Potash

Campl1gn

.,.

Compostie

of

North

&

South

evapora~

rs

Source of Water:

Water

that

condensed

in

tu.bes

ot

3rd eti'ect north

&

South

evaporators

ANALYSIS Silica SiO• Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid

so.

Carbonic Acid C03

Potassium

K

General Supt.

General Chemist

Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory Part> Pe< I 00,000

.34

oai

lo56

028 llo7l

6036

2G.45

.,)

7.83

8

46

57.38

29.78 87 .. 16

~

Chloride

~ ~

Potassium SU1phate

"Sodium Su'Ii,hate Na2S04 Sodium Carbonate Na2C03 Magnesium Chloride MgCl Magnesium Sulphate MgS04 Magnesium Carbonate MgC03

Calcium Chloride CaCl2

Organic and Volatile (by difference) TOT AL SOLIDS

_.,_

Parts Pu I 00,000

034 12o37

2~:ij

7,.74

3o90

.

41)81

Chief Chemi,-t.

(10)

-_ -_

_ _.Lo_.,n~£,OO-nt

_

Factory

_

J92Q_____

Kind of Water:

Drips from 4th effect evaporators.

Aver&Ge Sample

for the

potash Campaign - Composi ta

o'.t

!!ort-'11

&

South Evaporators

Source of Water:

Water that oandensed in tubes of 4th effect North

&

Sou th evaporators.

ANALYSIS

Silica

SiO• Iron Fe Calcium Ca Magnesium

Mg

Sodium Na Chlorine Cl

Sulphuric Acid

so.

Carbonic Acid C03

Potassium

K

Organic and Volatile (by difference)

TOT AL SOLIDS COPIES TO

General Supt.

General Chemist Asst. Genl. Supt.

Asst. Chief Engineer

Superintendent Parta Per 100,000

.36

.21

445 .27

13.27

6.56

13.73

12.00

7.50

•

55.35 23~09

78.44

HYPOTHETICAL COM8INA TIONS

Silica Si02

Potassium Chloride

lab1@d11ile

1lbmll

~otassium sulphate

odium Sulphate Na2S04 Sodium Carbonate Na2C03

Magnesium Chloride MgCI Magnesium Sulphate MgS04 Magnesium Carbonate MgC03

Calcium Chloride CaCl2

Calcium Sulphate CaSO,

Organic and Volatile {by difference) TOT AL SOLIDS Pam Per l 00.000

Analysis of water samples saved during the potash campaign of 1919-20

0

Thi. UilliAl1

WE

STERN SUG

A

H COl'L? ;.,NY

LOUGMOl?:.'

?AC~O...'W

..tt.liALYSIS OF WA'.::ER SA!.lPLES SAVED 1 ... UNG

'l.'HE POrASH CAJl.~!.IuH OF 1919

-

20

Copies to:

General Supt.

-

General Chemist,

Asst, Chief Engineer.

Superintendent,

Traveling Chemist.

Laboratory.

y

\'later

from Boiler

Feed Tank

'7

Water used

1n

washing

Hot

Presses

Legpipe

Water

from

1st

Condenser

or

North Evaporators

Legpipe Water from 1st Condenser ot South Eva:porat.Olrs

(

Drips

from 1st 'Ef'feot Jwa.porators

)

Drips fron 2dn 'Effeot Evatx>rators

/

Drips from 3rd Efteot EvaporatOJta

\

Drips from 4th Effect Evaporators

1

3

4

5

6

7

8

WATER ANALYSIS

I.ongm.ont

. _

_

Factory

May 21

192__o__

Water ~rom Boiler

Feed Tank

Average sample for the Potash Campaign

Drips from steam chamber of 2nd effect evaporators, and occasionally city water

so.

co

.

Ponasiwn

K

026

.20

lol3

.17

004

1.03

5.38

e33

2e69

_{May 21}

_{192o}

_{Drips from steam chamber of 2nd effect evaporators, and occasionally city water}

_{Drips from steam chambers of 3rd,}

_4th,

_&

_5th

_{ettect evaporators}

_~so

_{Vapor condensed in 1st condenser}

_or

_{north evaporator}