Analysis of water samples for the campaign 1921-22 Billings factory

(1)

r

t

ANALYSIS

OF

WATER SAMPLES FOR THE

CAMPAIGN

1921-22.

Copies to:

General

S

upt.

General Chemist.

'

-Asst. Genl. Supt.

Asst. Chief Engine

~

r.

Superintendent.

Traveling Chemist.

Laboratory.

BILLINGS

FACTORY

THE GREAT WESTEBN SUGAR COMPANY

(2)

, , I

KlllD

OF WATER

PAGE

YELLOWSTONE RIVER

l

CITY

2 MAIN

T.ANK

3 BATTERY

Sff

?

PLY (SmGLE SYSTEM)

4 H<Yr

PRES

S

WASH

5 COLD

SACCHARATE PRESS WASH

6 EVAPORATOR CONDENBER TAIL

PIPES

7 PAN

CONDENSER

TAIL PIPES

8 BOILER FEED

TANK

9 BOILER FEED (RETURN DIRECT)

10 FROM BOILERS

11

(3)

Form 443 2½m 9-21 Pad, 100

WATER ANALYSIS

THE GREAT WESTERN SUGAR COMPANY

B

I

L

I

N G

S

____ _

Factory

---=De=o=em=b~

e=r~,

-=

15 =

,

,,_

_ _ _

192~

Kind of Water:

YELLOWSTONE RIVER.

Description of Sample:

Average

sanple tor

the campaign. Sample

taken

from

the

intake

pump.

Source of Water:

Y

ellowstone

River water. Factory intake about

one

mile south

of

the faotory.

ANALYSIS Silica SiOz Iron Fe Calcium

Ca

Magnesium

Mg

Sodium

Na

Chlorine Cl Sulphuric Acid S04 Carbonic Acid C03

Organic and Volatile (by difference) TOT AL SOLIDS COPIES TO

General Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory

HYPOTHETICAL COMBINATIONS

Part. Per l 00.000 Parto Per 100.000

1.92

Silica SiOz

1.92 .11

Sodium Chloride NaCl

1.95

4.73

Sodium Sulphate Na2S04

10.38

1.76

Sodium Carbonate Na2C03

4.13

Magnesium Chloride MgCI

1.18

Magnesium Sulphate MgS04

8.32

13.66

Magnesium· Carbonate MgC03

.28

7.40

Calcium Chloride CaCI2

Calcium Sulphate CaS04

Calcium Carbonate CaC03

_11.81

Ferrous Carbonate FeC03

.23

34.89 _34.89

1.83

Organic and Volatile (by difference)

1.83

36.72

TOT AL SOLIDS

36.72 Page

1.

(4)

Form 443 2'/2m 9-21 Pod, 100

WATER ANALYSIS

:BILLINGS

_{_}

_Factory

_{____}

_{__.}

_{D~e~c~a~rollib~e~r..____.1u5~,-}

_{- - -}

_{192i__}

Kind of Water:

CTITY

WATER.

Average sample

for

the oampaign.

SourceofWater:

Yellowstone River. Water previously filtered

through

city

filtering

plant.

ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium

Mg

Sodium Na Chlorine Cl Sulphuric Acid S04 Carbonic Acid C03

TOT AL SOLIDS

COPIES TO General Supt. General Chemiot Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory Part, Per 100,000

1.44 .14

4.57 1.ao

3.89

1.00

13.07

7.43

33.42

2.70

36.12 Page

2.

HYPOTHETICAL COMBINATIONS Silica Si02

Magnesium Chloride MgCl

Magnesium Carbonate MgC03

Calcium Chloride CaClz

TOT AL SOLIDS Pam Per 100,000

1.44

1.78

9.85

8.03 .62

11.41 .29

33.42

2.70

36.12

Chief Chemiot.

(5)

Form 443 2½m 9-21 Pad, 100

WATER ANALYSIS

_ _ _

B

_

I

_

L ~_!_U S

_

Factory

- - -

--'D=-eo=e=m=ib,._,e=r'----"'l=5_..,

_ _ _

J

92----1.L_

Kind of Water: Description of Sample: Source of Water: Silica Iron Calcium Magnesium Sodium Chlorine Sulphuric Acid Carbonic Acid

MA.IN TANK.

Average sample for the

oa.mpaign.

Yellowstone River water. Also possible to send city water. Main

source of supply for all factory operations.

ANALYSIS HYPOTHETICAL COMBINATIONS

Pam Per 100,000

Si02

_1.64

Silica SiOz

Fe

_.07

Ca

4.36 Mg

1.66

Na

5.40

Cl

_1.18

Magnesium Sulphate MgS04 504

_14.90

Magnesium Carbonate MgC03 C03

7.45

Calcium Chloride CaCl2

36.66

Organic and Volatile {by difference)

2.62

Organic and Volatile {by difference) TOT AL SOLIDS

COPIES TO General Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory

39.28

TOT AL SOLIDS

Page 3.

Part, Per 100,000

1.64

1.95

14.30

6.55

1.18

10.89 .15

36.66

2.62

39.28

Cbie/Chemiot.

(6)

Form 443 2½m 9-21 Pad, 10()

WATER ANALYSIS

_ _

_

B

_

I

_

L L I

N G S

_ _ _

Factory

_ _ _ _ _

D_e_o

_

e

_

m

_

b

_

e

_

r

_

l

_

5 _

,

_ _ _

_192~

Kind of Water:

BATTERY SUPPLY

(

SING

L

E SYSTEM

)•

Average sample for the

eampaign.

Source of Water:

All water

from tail

pipes of the upper condensers

of

the evanorators,

and

dri

ps

from

vapor

pan. Possible to

semd

water from

the

main

tank.

ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid 504 Carbonic Acid C03

TOT AL SOLIDS

COPIES TO General Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory Paru Per I 00,000

1.24 .17

2.29

1.26

3.28 .98

9.71

4.10

23.03

4.17

27.20 Page 4.

HYPOTHETICAL COMBINATIONS Silica Si02

Organic and Volatile {by difference)

TOT AL SOLIDS Pam Per I 00,000

1.24

1.62

8.15

5.26 .69

5.72 .35

23.03

4.17

27.20

Chief Chemi.t.

(7)

Form 443 2½m 9.21 Pad, IOQ

WATER ANALYSIS

B I L L I N G S

_{_}

_Factory

-

---=D~e=c=em

=

b=e=r~l=5~,

___

192l..!_

-

-Kind of Water: Description of Sample: Source of Water: Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium

Na

HOT PRESS WASH.

Average sample for the

campaign.

Condensed

water from the

first effeot of the evaporators,

battery

calorisators,all heaters, and

overfl01J ~rorn

the

boiler feed

tank.

Possible

to

bypass battery

supply

to

press

wash

and send

drips from all

evaporators, carbonation and bl0Wl%,P traps and office

heating system.

ANALYSIS HYPOTHf::TICAL COMBINATIONS

Pam Per 100,000 Pam Per 100,000

.24

Silica Si02

.24

.11

.64

.33

.09

.10

.28

.39

.49

.66

.48

.30

. Calcium Carbonate CaC03

.60

.23

2.59

4.15

TOT AL SOLIDS

6.74

TOT AL SOLIDS

6.74 Page

5

1

(8)

Form 443 2½m 9-21 Pad, 100

WATER ANALYSIS

BILLINGS

_{_}

_Factory

_____

D

_

e_ce_mb

_

e

_

r

_

l

_

5~,

_ _ _

l9Z~

- - - -

-Kind of Water: Description of Sample: Source of Water: Silica Si02 Iron Fe Calcium Ca Magnesium

Mg

Sodium Na Chlorine Cl Sulphuric Acid 504 Carbonic Acid C03

COLD SACCRARATE PRESS WASH.

Average sample tor the campaign.

City

water.

Pam Per 100,000

1.52

Silica Si02

.14

Sodium Chloride NaCl

4.72

1.66

4.09

1.37

12.92

7.42

Calcium Chloride CaCI2

Calcium Sulphate CaS04

33,84

3.54

TOT AL SOLIDS

37,38

TOT AL SOLIDS

Page 6.

Pam Per I 00,000

1.52

2.26

9.88

7.82 .28

11,79

,29

33.84 3J54

37.38

Chief Chemiot.

(9)

Form 443 2½m 9-21 Pad, IOQ

WATER ANALYSIS

_

___

B I L_L

LN

G_

S

_

_{_}

_Factory

_{_____}

_D

₌

_e=c=e

₌

_m

₌

_b

_~

_e

₌

_r--=1

₌

_5~,

_{___}

_192~

Kind of Water: Description of Sample: Source of Water: Silica Iron Calcium Magnesium Sodium Chlorine Sulphuric Acid Carbonic Acid

OC!IDENSER TAIL PIPES OF EVAPORATORS.

Average sample for

the

oanipaign.

Main water tank, main source of supply foe all factory operations.

Part, Per I 00,000

Si02

1.76

Silica Si02

Fe

.11

Ca

4.37 Mg

1.65 Na

4.26

Cl

1.1a

S04

12.37

C03

7.60

Calcium Sulphate CaS04 Calcium Carbonate CaC03

Organic and Volatile (by difference}

33.30

2.30

Organic and Volatile (by difference} TOT AL SOLIDS

~5.60

TOT AL SOLIDS

Page 7.

Par11 Per 100,000

1.76

1.95

10.78

6.35

1.32

10.91 .23

33.30

2.30

35.60

Chief Chemist.

(10)

Form 443 Z½m 9-21 Pad, 100

f

WATER ANALYSIS

BILLINGS

_{_}

_factory

_ _ _ _ _ _

D

_

e

_

o

_

e

_

mb

_

e

_

r

_

l

_

S

_

,

_ _

_192~

Kind of Water: Description of Sample: Source of Water: Silica SiOz Iron Fe Calcium Ca Magnesium

Mg

CONDENSER TAIL PIPES OF .ALL P.ANS.

Average sample for

the oaJ'!I!'.)aign.

Main water tank, main source of supply for all factory operations.

ANALYSIS Pam Per I 00,000

1.76 .13

3.62

1.59

4.16

1.47

9.40

7.81

29.94

9.12

HYPOTHETICAL COMBINATIONS Silica SiOz

Calcium Chloride CaClz

F enous Carbonate FeC03

Part, Per 100,000

1.76

2.42

9.91

3.38

3.16

29.94

9.12

TOT AL SOLIDS

_39.06

TOT AL SOLIDS

39.06

COPIES TO General Supt. General Chemist

Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist

Laboratory

Page

a.

(11)

Form 443 2½m 9.21 Pad, 100

WATER ANALYSIS

B I

L L

I

N

G

S

____

factory

_{- - - -}

_{-=D~e~ce~m~b=e=r,.__.,,1~5~,-}

_{- -}

_192~

Kind of Water: Description of Sample:

Source of Water:

WATER F

R

OM BOILER FEED TANK.

Average sam~le for

the campaign.

Drips from

2nd, 3rd,4th,

and

5th.

bodies of

the eva

n

orators, all

live

steam, all granulators, all

heating

systems, 1st, 2nd,

and

3rd, condensers and blowup

traps.

Possible to send

drips

from

all heaters

to

boiler

teedo

Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium

Na

Organic and Volatile (by difference) TOT AL SOLIDS COPIES TO

General Supt. General Chemist Asst. Genl. Supt. Asst, Chief Engineer Superintendent Traveling Chemist Laboratory

Part, Per I 00,000 Pam Per 100,000

.14

Silica Si02

_.14

.11

Sodium "Chloride NaCl

_.56

.17

.so

.09

.48

.34

_.45

1.15 .22

_.35

.17

F enous Carbonate FeC03

.23

2.70

2.70 .30

.30

3.00

TOT AL SOLIDS

_3.00

Page

9

₁

(12)

Form 443 2½m 9-21 Pad, JOO

WATER ANALYSIS

BILLINGS

_{_}

_Factory

_-

_{--~De~ce=m=b~e~r~l=5}

_~,

_{_ _}

_{__}

_{J92l..!__}

Kind of Water:

Description of Sample: Source of Water: Silica Si02 Iron Fe Calcium Ca Magnesium

Mg

Sodium

Na

Chlorine Cl Sulphuric Acid S04 Carbonic Acid C03

BOILER

FEED

WATER

( RETURN DIRECT).

Average sample for the canpaign.

Condensed

water from all pan

ooils, except

vapor pan.

Pumped

direct

to

boilers.

Parts Per 100,000

.40

Silica Si02

.10

.11

.07

.45

.44

.64

.26

-2.47

.59

Organic and Volatile (by difference) TOT AL SOLIDS

3.06

TOT AL SOLIDS

Page

10.

Parts Per 100,000

.40

.73

.49

.35

.04

.25

.21

2.47 .59

3.06

Chief Chemiot.

(13)

Form 443 Z½m 9-21 Pad, 10()

BILLINGS

-Kind of Water: Description of Sample: Source of Water:

WATER ANALYSIS

____

factory

_{- - - - ~}

_{D~e~c~em-~~e~r.__..l-5~,}

_{- - -}

_{192_i.__}

FROl BOILERS.

Average sample for the campaign.

Water from boiler feed

tank

and from condensed waters from pan coils

pumped direct to boilers.

Silica SiOz Iron Fe Calcium Ca Magnesium

Mg

TOT AL SOLIDS

COPIES TO General Supt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory Pam Per 100,000

1.24 .20

.90

.oa

35.54

2.75

22.06

32.02

94.79

37.21

132.00 Page 11.

Part, Per I 00,000 Silica SiOz

_1.24

Sodium Chloride NaCl

_4.53

32.62

53.46 .28

Calcium Chloride CaCiz

2.25 .41

94.79

37.21

TOT AL SOLIDS

_132.00

(14)

'r ,

,t

_,.,

_,.,.

. d'. ~ I

(

t

Q

,(1~ ~ '- J...