Analysis of waters for campaign 1949-1950 Billings factory

(1)

CC:

ANALYSIS OF WATERS FOR CAMPAIGN

1949-1950

BILLINGS FACTORY

THE GREAT WESTERN SUGAR COMPANY

General Chemist

/

Assistant General Superintendent

(2)

INDEX

KIND OF WATER

MAIN TANK (RIVER WATER)

CITY

WELL

BATTERY SUPPLY

PRESS WASH

CENTRIFUGAL WASH

COLD SACCHARATE CAKE

BOILER FEED

BOILER

PAGE

1

2 .3

4

5

6

7

8

9

(3)

Form 443 -2M-8-48 -Pads 100

WATER ANALYSIS

___

_

___ ;I?.

_

): ___

~

__

}:,

_

J _

_

~

__ g

__

§.

____

_

__

_

__

Factory

_{__________ ·}

_{____________}

_April

_{_}

17 ,

_________________

_

____

₁₉___

50 _

Kind of Water:

River

W

ater

Description of Sample:

_{Average Sample for Campaign}

_1959-50

pH 8.

2

Source of Water:

_Ye

_ll

_{owstone River}

Intake one mile sou

t

h of

f

actory

ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulfuric Acid

so,

Carbonic Acid

co.

Phosphoric Acid PO,

Organic and Volatile (by difference)

TOTAL DISSOLVED SOLIDS AT 105° C

COPIES TO

General Chemist Asst. General Supt, District Engineer Superintendent Laboratory

pH

Parts Per Million

18o0

2.5

44.0

18.4 4lol

10.1

132.5

65.1

331.7 31119

6 6

HYPOTHETICAL COMBINATIONS Silica Si02

Sodium Chloride NaCl

Sodium Sulfate Na.SO,

Sodium Carbonate Na2COs Sodium Phosphate NasPO, Magnesium Chloride MgCI.

Magnesium Sulfate MgSO,

Magnesium Carbonate MgCOs

Magnesium Phosphate Mgs(P0,)2

Calcium Sulfate CaSO,

Calcium Carbonate CaCOs Calcium Phosphate Cas(PO,). Ferrous Carbonate FeCOs Ferrous Phosphate Fea(PO,).

--=

Parts Per Million

1s.o

16.7

106.6

75.7

10.7

98.8

5.2

331.7 31,9

(4)

Form 443- 2M-8-48- Pa.ds 100

WATER ANALYSIS

..

.

..

.

..

. B

.

. 1

.

. 1

.

. L .. l .. N

..

. G

...

S ..

.

....

...

..

.

Factory

.

...

April

.

. 17-,

...

.

...

19 .

50 ..

.

Kind of Water:

_{City Water}

_Avera

_·

_{ge Sample for Campaign 1949-50}

pH

8.25

Source of Water:

_,

_{River water}

_{treated and filtered thru City Water Plant}

Sulfuric Acid

so.

Carbonic Acid

co.

Phosphoric Acid PO,

COPIES TO

General Chemist Asst. General Supt. District Engineer Superintendent Laboratory

pH

Parts Per Million

17.0

2.0

50.6

16.3

32.9

11.8

112.3

79.0

2.0

32.3.9

5.5

-2-HYPOTHETICAL COMBINATIONS Silica Si02

Sodium Carbonate Na2COs

Sodium Phosphate NaaPO,

Magnesium Chloride MgCb

Magnesium Carbonate MgCOa Magnesium Phosphate Mga(PO,).

Calcium Carbonate CaCOs

Calcium Phosphate Caa(PO,).

Ferrous Carbonate FeCOa

Ferrous Phosphate Fea(PO,),

17.0

19.5

77.8

126.4 .4

3.8

323.9

5.5

TOTAL DISSOLVED SOLIDS AT 105° C _ _ _ ,_,,29_..JJ,

(5)

Form 443-2M-8-48 -Pads 100

WATER ANALYSIS

....

...

~

.

J. ..

k

.

k

.

l.: .

.

N

.

. 9

...

$. .

...

.

....

Factory

.

....

.

...

.

...

.

..

!P~J .

..

~!J

...

.

...

.

19 ...

.?.9 .

.

Kind of Water: Description of Sample: Source of Water:

Well Water (Used for Cold Sacch.

W

ash)

Average Sample for Campaign 1949-50

pH

8.2 -We

l

l located south and ad

j

acent to lime rock hopper

ANALYSIS HYPOTHETICAL COMBINATIONS

Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulfuric Acid

so.

Carbonic Acid

co.

Phosphoric Acid PO,

COPIES TO General Chemist Asst. General Supt, District Engineer Superintendent Laboratory pH.

Parts Per Million

26.0

Silica Si02

2.3

53.3

Sodium Sulfate Na2SO,

35.3

Sodium Carbonate Na2COa

145.4

Sodium Phosphate Na,PO,

19.S

Magnesium Chloride MgCI.

301.2

154.1

Magnesium Carbonate MgCOa

Magnesium Phosphate Mga(PO,). Calcium Sulfate CaSO, Calcium Carbonate CaCOa Calcium Phosphate Caa(PO,). Ferrous Carbonate FeCOa Ferrous Phosphate Fea(P0,)2

73704

38.6 _ _

.,.__

7,6

...,

0 ,.__

.,..

_

g,;L

Parts Per MilJion

26.0

32.6

409.5

30.5

100.9

133.1

4.8 73704

38.6

(6)

Form 443-2M-8-48-Pads 100

WATER ANALYSIS

...

..

...

B

...

I

..

L

..

.L

..

I ..

N

...

G. ..

S .

.

..

...

.

..

.

Factory

.

...

~.Pr:ti

..

J'.7

.

,

..

.

...

.

..

19 .

.5-9 ...

.

Kind of Water:

_Battery

_Supply

_{Average Sample}

_{for Campaign}

_1949-50

Source of Water: ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulfuric Acid

so,

Carbonic Acid

co.

Phosphoric Acid PO,

COPIES TO

pH

HYPOTHETICAL COMBINATIONS

Parts Per Million

12.s

Silica Si02

2.4

33.7

15.0

32.4

Sodium Pho·sphate NaaPO,

9.2

96.3

64.4

Magnesium Phosphate Mga(PO,). Calcium Sulfate CaSO,

Calcium Carbonate CaCOs

Calcium Phosphate Caa(P0,)2

Ferrous Carbonate FeCOa Ferrous Phosphate Fes(P0,)2

266.2 l,4.2

280._l+

_ _

9.

I

12.s

15.2

81.5

84.1

5.0

280.

Chief Chemist.

(7)

Form 443- 2M- 8-48- Pads 100

WATER ANALYSIS

..

.

..

.

..

.

.. :e.

.

I .

.

k .

.

J:.

.

I

.

N

..

.G

.

..

S. ..

..

.

...

.

Factory

_...

_{Apr.tl. .}

_.

_l

_.

_7.,-

_..

_...

_..

_.

_..

19 .

.5.Q

.. .

Kind of Water: Description of Sample:

Source of Water:

Press Wash

Average Sample for Campaign 1949-50

Condensed waters from all 1st effect evaporators, battery

calorisators, all heaters and overflow from boiler feed.

Possible to send battery supply to press wash, arxi drips

from all evaporators and blow-up traps

Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulfuric Acid

so,

Carbonic Acid

co.

Phosphoric Acid PO,

COPIES TO

pH

Parts Per Million

_ _

'27..

0

Silica SiO,

Sodium Sulfate Na,SO,

Sodium Phosphate Na.PO,

Magnesium Chloride MgCl2

Magnesium Phosphate Mgs(PO,).

Calcium Carbonate CaCO,

Calcium Phosphate Cas(PO,).

Ferrous Carbonate FeCOa

Ferrous Phosphate Fes(P0,)2

(8)

Form 443-2M-8-48- Pads 100

WATER ANALYSIS

..

...

.

... J~ ..

.l ...

l.!

.

t

..

l .

.

N

.

. JLS ..

.

..

.

..

Factory

_...

_.

_....

_.

_...

_{.. Aptil .}

_.

_17~

_...

_.

_..

_...

19 ..

.5.9.

..

Kind of Water:

Water used to wash white sugar

_{Average Sample for Campaign 1949-50}

Source of Water:

_{Drips from steam chest of the 3rd effect of north evaporators}

ANALYSIS Silica SiO, Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulfuric Acid

so.

Carbonic Acid

co.

Phosphoric Acid PO,

COPIES TO

pH

Parts Per Million

28.o

Silica Si02 Sodium Chloride NaCl Sodium Sulfate Na,SO, Sodium Carbonate Na2COa Sodium Phosphate Na.PO, Magnesium Chloride MgCI. Magnesium Sulfate MgSO, Magnesium Carbonate MgCOa Magnesium Phosphate Mg.(PO,)s Calcium Sulfate CaSO, Calcium Carbonate CaCOs Calcium Phosphate Caa(PO,). Ferrous Carbonate FeCOs Ferrous Phosphate Fes(PO,),

_28.0

(9)

Form 443-2M-8-48-Pads 100

WATER ANALYSIS

... ?.

..

J ... ~.-~.} ..

~

.

.?

...

~

...

....

Factory

...

....

April

..

17,

...

.

..

...

....

..

....

! 9 ..

50 ..

Kind of Water:

_Cold

_Saccharate

_{Wash Water}

_{Average Sample}

_for

_{Campaign 1949-50}

See

Page

-3-Source of Water:

_{Well Water}

ANALYSIS Silica SiO, Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulfuric Acid

so.

Carbonic Acid

co.

Phosphoric Acid PO,

COPIES TO

General Chemist Asst. General Supt, District Engineer Superintendent Laboratory

pH

Parts Per Million

Silica Si02

Sodium Carbonate Na,COs Sodium Phosphate Na,PO, Magnesium Chloride MgCl2 Magnesium Sulfate MgSO, Magnesium Carbonate MgCOa Magnesium Phosphate Mgs(PO,). Calcium Sulfate CaSO, Calcium Carbonate CaCOs Calcium Phosphate Caa(PO,). Ferrous Carbonate FeCOa Ferrous Phosphate Fes(PO,),

(10)

Form 443 -2M-8-48- Pads 100

WATER ANALYSIS

BILLINGS

... Factory

...

.

...

.-!\p.r.il

..

17,

...

.

....

.

....

.

...

19 ..

.50

..

Kind of Water:

_{Water in Boiler Feed Tanlc}

_{Average Sample}

_for

_{Campaign 1949-50}

Source of Water:

_{Drips from 2nd,}

_3rd,

_4th

_&

_{5th bodies}

_{of evaporators}

Drips from pans

after flashing to exhaust. All

live steam

traps

Sulfuric Acid

so.

Carbonic Acid

co.

Phosphoric Acid PO,

COPIES TO

pH

Parts Per Million

24.0

Silica SiO,

Sodium Carbonate Na,COa

Sodium Phosphate Na,PO,

Magnesium Carbonate MgCOs Magnesium Phosphate Mgs(P0,)2

Calcium Carbonate CaCOs Calcium Phosphate Cas(PO,). Ferrous Carbonate FeCOs Ferrous Phosphate Fea(P0,)2

_24.0

(11)

Form 443- 2M-8-48-Pads 100

WATER ANALYSIS

..

.

...

.

?. ..

J ..

J,_J~ .. .+. .

.

N

.

G. ..

~

.

...

.

....

Factory

_...

_....

_Apri.l

_...

_l7.

_,

_...

_.

_...

I9 ...

50 ..

Kind of Water: Description of Sample: Source of Water:

- - - ~ = ~

Water in Boilers

Average Sample for Campaign

1949-50

Added

to Boilers: Caustic

Soda

Calgon

Sod.

Sulphite

Alkalinity

Hardness

Po

₄

Pounds

For Camp.

3315

807

228 Per

Day

44.8

10.9

3.1

Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulfuric Acid

so.

Carbonic Acid

co.

Phosphoric Acid PO,

Organic and Volatile (by diffel'ence)

COPIES TO

pH

Parts Per Million

7.0

2.1

1.7

322.3

18.5

83.0

322.5 74o0

831.1 5J.4e9

Silica Si02

Sodium Chloride NaCl Sodium Sulfate Na2SO, Sodium Carbonate Na.COs Sodium Phosphate Na,PO, Magnesium Chloride MgCI. Magnesium Sulfate MgSO, Magnesium Carbonate MgCO, Magnesium Phosphate Mgs(P0,)2 Calcium Sulfate CaSO, Calcium Carbonate CaCOa Calcium Phosphate Ca,(PO,). Ferrous Carbonate FeCO, Ferrous Phosphate Fea(P0,)2