Analysis of water samples for the campaign 1920-1921 Gering factory

(1)

MITQWliHc FAQTQRY

~fCBVtb

. MAR 16

19~1

&EN'l CH-EM'S OFflC

F

G, W. S.

CO.

Analysis ot Water Samples Sava4 During 0~1gn 1920•1921

Oop1es

to;-General

Sup

.

• t.

General

Chemie.-Ass

.

' t. Gen'l.

Sup

.

•t

Ass.'t. Chief l!lngineer

Superintendent

fravel1ng Chemist,

Laboratory,

(2)

X1n4 at later

.

!lain

Water

SupplY•••••••••••••••••••••••••••ol

.Battery Supply

Pure••••••••••••••••••••••••••2

Battery Supply Impure••••••••••••••••••••••••3

Water

From Boiler Feed

Tank••••••••••••••••••'

Water

In Boilers•••••••••••••••••••••••••••••5

Hot

Presa

Wash••••••••••••••••••••••••••••••o6

First

Evaporator Condenser Lag Pipe

saa1 •••••

7 Seoond :m.raporator Oondanaer Leg Pipe

Saa1 ••••

a

Water

From Condenser Leg Piper Of All

Pans ...

9

(3)

Kind of Water: DescriptiGn of Sample:

THE GREAT WESTERN SUGAR COMPANY

__ _

Factory

J4A.IN WATER SU.PPLY

Average Sample for

Gampaign

__

192 _

1 _

Source of Water:

_{From a drainage ditch which oa.rriea aeepwater trom swamp land to the River.}

The Factory

~pply

intake located about one mile west of the

Factory•

ANALYSIS Silica SiO• lroa Fe Cll!icium Ca Magnesium

Mg

Sodium Na Chlorine Cl Sulphuric Acid S04

Carbonic Acid

co.

Organic and Volatile (by difference)

TOT AL SOLIDS

COPIES TO General Supt.

General Chemist Aost. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory Part. Pe< 100,000

5.50 .30

5.14

1.16 s.49

1.90 -

5.35

10.49 3S.33

la51

34.84

HYPOTHETICAL COMBINATIONS Silica Si02

Sodium Chloride NaCl Sodium Sulphate Na2S04 Sodium Carbonate Na2C03 Magnesium Chloride MgCI Magnesium Sulphate MgS04 Magnesium C~bonate MgC03

Calcium Chloride CaCl2

Calcium Sulphate CaS04

Calcium Carbonate CaC03 Ferrous Carbonate FeC03

Organic and Volatile (by difference) TOT AL SOLIDS

(1)

Parts Pei I 00,000

5.50

3.13

6.98 .79

3.47

12.84 e62

33.33 la51

34.a,

(4)

_

factory

BATTERY SUPPLY

POim

Average Sample tor

Campaign

_192..i_

Source of Water:

Overflow :f'rom Preas

Wash

and overflow form

seal

_{First lllrndensed}

_Leg

_Pipe

ot

the Evaporator,

ANALYSIS Silica SiO. lroa Fe Cai!cium Ca Magn~um Mg Sodium Na Chlorine Cl Sulphuric Acid S04

Carbonic Acid

co.

TOT AL SOLIDS

COPIES TO

General Supt. General Chemist Asst. Genl. Supt. AS!!t. Chief Engineer Superintendent Traveling Chemiot Laboratory Part, P« 100,000

4.1,

.43

,.23

1.31

3.00

1.90

5.63 8,81

29,4.5

2~85

32.30 (2)

HYPOTHETICAL COMBINATIONS Putt Per I 00.000 Silica Si02

4.1,

Sodium Chloride NaCl

_3.13

Sodium Sulphate Na₂S0₄

_5.47

Sodium Carbonate Na2C03

Magnesium Chloride MgCl

Magnesium Sulphate MgS04

2,42

Magnesium Cl'.\fbonate MgC0₃

_2.84

Calcium Sulphate

easo.

Calcium Carbonate CaC0₃

_10,56

Ferrous Carbonate FeC03

,89

29,45

2.as

TOT AL SOLIDS

_32,30

,

/Oif~

/ / , v

f /

· r 7 ~

__

,

__

(5)

Kind of Water: Description of Sample:

Factory

BATTERY SUPPLY

Da'tJ.RB

Average Sample

tor

Campaign

_

J92_l_

Source of Water:

Overtlow trom Battery

Supply

Pure

and

OTertlow trom Evaporator

and

Pan

S e a l ~

ANALYSIS Silica SiO, lroa Fe Cadcium Ca Magne11ium Mg Sodium Na Chlorine Cl Sulphuric Acid 504

Carbonic Acid

co.

Organic and Volatile (by difference} TOT AL SOLIDS COPIES TO

Genrral Supt. General Chemist A9St. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory Pam Pee I 00,000

3e'12

.10

'·'"

.92

4.6'

1.20

7.65

9.27

31.94 3t08

35.02 (3)

HYPOTHETICAL COMBINATIONS Parts Per 100,000 Silica SiO,

_3.'12

_lc98

Sodium Sulphate Na2S04

11.31 .46

Magnesium Chloride MgCI

Magnesium Cap:bonate MgC03

3.17

Calcium Sulphate

easo.

Calcium Carbonate CaCOa

_11.09

.21

31.94

Organic and Vohrtile lby difference}

a.oe

TOT AL SOLIDS

_35.02

(6)

-THE GREAT WESTERN SUGAR COMPANY

MITQHELJ.

__

_factory

WATER FROK BOILER

FEiiID

TANK

Average Sample tro

Out,aign

Jlarch,

_10

Source of Water:

Drips trom Coils

ot

White Pan, trom0alandriaa

ot

the

Baw

Pana,

and

f'rom

the Stum

Oh.ambers of'

2nd,

3rd, 4th,

&

5th, Ettectao

ANALYSIS Silica Si02 lroa Fe Cailcium Ca Magnelium Mg Sodium Na Chlorine Cl

Sulphuric Acid

so.

Carbonic Acid

co.

Organic and Volatile (by diffetence)

TOT AL SOLIDS

COPIES TO Gen~ral Supt.

General Chemist A9llt, Genl. Supt.

Asst. Chief Engineer

Superintendent Traveling Chemist Laboratory Part, P« 100,000

1.95 .09

2.10 .26

.46

.60

2.30

2.54

10.30 l.78

12.oa

HYPOTHETICAL COMBINATIONS

Silica Si02

Sodium Carbonate Na.C03

Magnesium C.,bonate MgC03

Calcium Carbonate CaCO"

Ferrous Carbonate FeC0₃

Organic and Volatile thy difference) TOTAL SOLIDS

(4)

_192_1_

__

PartJPer~.

1.95 .99

.22

1.29

1.59

4.07 .19

10.30 l.78

12.08

(7)

_ _ __ _,llI_TQHET..., _ _

.r_.

___

_

__.

_

Factory

_{Karch, 10}

Kind of Water:

_'D!l!ER

_{IN BOILERS}

DescriptiGn of Sample:

_{Ayerage Sample tor Oampaign}

Source of Water:

_Water

_{actually in the Boilers}

ANALYSIS _{HYPOTHETICAL COMBINATIONS}

Silica Si02 lroa Fe Calcium Ca Magn~ium Mg Sodium Na Chlorine Cl Sulphuric Acid S04 Carbonic Acid C03

TOT AL SOLIDS

COPIES TO Genrral Supt. General Chemitt

Asst, Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory Parta Per I 00,000

5.42 .69

17.77

3.56

43.86

4.30

32.62

69.33

177.55

104.45

282.00

Silica Sio2

Magnesium Sulphate MgS04 Magnesium C'¥bonate MgC03 Calcium Chloride CaCl2 Calcium Sulphate CaS04 Calcium Carbonate CaC08 Ferrous Carbonate FeC03

Organic and Volatile (by difference) TOT AL SOLIDS

(5}

__

192-1.

_

Part• Per 1_00,000

5.42

7.09 '8.24

58.65

12.34

44.38

1.43

177.65 10,.4.5

282.00

(8)

WATER ANALYSIS

Factory

HOT PBESS

\VJ.SR

- - - · · -

__

Var.oh,

__

10 . ___

192..1

_

Kind of Water:

Description of Sample:

_Average

_{Sample tor C8DU)&ign.}

Source of Water:

_{Overflow from Boiler Feed}

_Tank,

_{Drips trom ~ck Juice Heaters,}

lat.

2nd,&:

3rd, Carb.

H

eaters, Thin Juice

H

eater,

Ba,

Juice Heaters, lat. Etrect

Steam Chamber, lat, 2nd,

&

3rd, Oarb.

&:

Blow-up Steam Coils, Upper Granulator

Steam Ooila, Pan Storage Tank Coils, and Battery Oalorizatora.

ANALYSIS HYPOTHETICAL COMBINATIONS

Parll Pe< 100,000 Parll Per 100,000

Silica Si02 lroa Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid

so~

Carbonic Acid C03

Organic and Volatile (by difference) TOT AL SOLIDS COPIES TO

General Supt. General Chemi AIIOt.

Genl.

Supt.

Aat.

Chief Engineer Superintendent Traveling Chemist Laboratory

2.30 .06

2.62 .50

.62

.90

2.30

3.82

13.12 1.aa

15.00 (6)

Silica Si02

2.so

1.48 ol2

2.47

Magnesium C.bonate MgC03

e36

Calcium Carbonate CaC08

6.27 .12

13.12 1.aa

(9)

_ _ _ _ _

__.MI~T""QHET

...

_.r __ .

_

____

_Factory

_{--- --- _}

_{Maroh, _}

_{~Q_}

_~

_{__}

_J

_{92!__}

_.

Kind of Water: Descriptie>n of Sample:

FIBS!!! EVAPORATOR 00:NDENSER LEG PIPE SEAL

{HOT

Lm)

Average

Sample tor Campaign

Source of Water:

_Water

_from

_{Main water}

_{supply after condensing vapors}

_in

_{the 1st. condenser}

ot

the

Evaporators

ANALYSIS Silica SiO, lroa Fe Ca,lcium Ca Magne9ium

Mg

Sodium Na Chlorine CI Sulphuric Acid S04 Carbonic Acid C03

Organic and Volatile {by diflereoce) TOT AL SOLIDS COPIES TO

Gen~al Supt. General Chemist-A .. t. Genl. Supt. Asst. Cbief Engineer Superintendent Traveling Chemist Laboratory Parts Pe< 100,000

4.94 .22

4.36

1.14

4.95

2.90

8.37

8.35

35.23

1.47

36.70

HYPOTHETICAL COMBINATIONS Part, Per 1_00,000 Silica Si02

4.94 _4.'78

9.48

Sodium Carbonate Na,C03

2.46

Magnesium c,.bonate MgC03

2.22

Calcium Chloride CaCI2

10.eg

Ferrous Carbonate FeCOa

_.46

35.23 _i.47

TOT AL SOLIDS

_36.70

(10)

_

Factory

_{_ _}

_{Karch, -10}

_

192___1_

_

Kind of Water: Description of Sample:

SECOND EVAPORlTOR 00:tmENSER

Lm

PIPE SEAL

( COLD

Lin)

Averag6 Sample tor 08.Dplign

Source of Water:

_{Water trom main water wupply attar condensing vapors in the}

_2nd.

_condenser

of the Bvaporatora.

ANALYSIS Silica Si02 lroa Fe Cailcium Ca Magrt$um Mg Sodium Na Chlorine Cl Sulphuric Acid S04 Carbonic Acid

co.

Organic and Volatile (by difference) TOT AL SOLIDS COPIES TO

General Supt, General Chemist A!l<lt. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory Parts P« 100,000

4.99 .11

s.20

1.17

5.62

3.20

8.62

10.03 se.94

1.91

40.85 (8)

HYPOTHETICAL COMBINATIONS Parts Per 100,000 Silica Si02

4.99 _5.28

10.93

Magnesium Sulphate MgSO.j

1.54

Magnesium c..,bonate MgC03

2.98

12.99 .23

se.94

_le91

TOTAL SOLIDS

_40.85

(11)

___

Factory

_Jlaroh.

₁₀

_{_}

192-1-Kind of Water:

WATER

FRO)(

CONDENSER LEG PIP:m OF

.ALL

PANS

Description of Sample:

Average Sample tor Campaign

Source of Water:

Water from

min water

au,pply

atter condenaing vapora, in

the

condensers

of all pans

ANALYSIS Silica Si02 lroa Fe Cadcium Ca Magne!lium Mg Sodium Na Chlorine Cl

Sulphuric Acid

so~

Carbonic Acid

co.

Organic and Volatile (by difference} TOT AL SOLIDS COPIES TO

Gen~al Supt. General Chemist Asst. Genl. Supt.

Asst. Chief Engineer Superintendent Traveling Chemist Laboratory Part, Per I 00,000

3.56 .31

2.75 .31

5.84

2.70

8.97 ,.94

29.38

3.54

32.92 (9)

HYPOTHETICAL COMBINATIONS Parts Per I 00.000 Silica Si02

_3.56

_4.45

_12.63

Sodium Carbonate Na2C03 Magnesium Chloride MgCI

.54

Magnesium Ci,:bonate MgC03

.69

Calcium Sulphate

easo,

6.87 _.64

29.S8

Organic and Volatile lby difference}

_~.5fi

(12)

_

Factory

W.A.fER FROM Pil SEAL

!U.NX

Average Sample tor Oampaig:n

_

March,

10

Source of Water:

Water from

pan

condenser leg pipes with some water trom leg pipes

of let.

&

2nd.

evaporator condensers.

ANALYSIS Silica SiO, Iron Fe Cllllcium Ca Magnaium Mg Sodium Na Chlorine Cl Sulphuric Acid

so.

Carbonic Acid C03

TOT AL SOLIDS

COPIES TO Genual Supt.

General Chemist _.,,.

A:!SI. Genl. Supt.

Parts Per I 00,000

5.20 .10

s.12

1.26

3.18 2.ao

8.60

7.28

33.54

1.66

35.20

HYPOTHETICAL COMBINATIONS

Silica Si0₂

Magnesium C..-bonate MgC03

Organic and Volatile (by difference}

TOT AL SOLIDS

_

1921_

Parts Per 1_00,000

s.20

4.62 ,.20

6.23

1.12

11.96 .21

33.54

1.66 as.20

Asst. Chief Engineer Superintendent Traveling Chemiot Laboratory