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A. Garcia-Carrasco , P. Petersson , M. Rubel , A. Widdowson , E. Fortuna-Zalesna , S. Jachmich

d

, M. Brix

b

, L. Marot

e

, JET Contributors

1

a Royal Institute of Technology (KTH), SE-10044 Stockholm, Sweden

b EUROfusion Consortium, JET, Culham Science Centre, Abingdon, OX14 3DB, UK

c Faculty of Materials Science and Engineering, Warsaw University of Technology, 02-507 Warsaw, Poland

d Laboratory for Plasma Physics, Ecole Royale Militaire-Koninklijke Militaire School, 10 0 0 Brussels, Belgium

e Department of Physics, University of Basel, Klingelbergstrasse 82, CH-4056 Basel, Switzerland

a rt i c l e i nf o

Article history:

Received 29 June 2016 Revised 29 November 2016 Accepted 27 December 2016 Available online 16 February 2017 Keywords:

JET

First mirror test Diagnostic mirrors Erosion-deposition

a b s t ra c t

Metallicmirrorswillbeessential componentsofallopticalsystemsforplasmadiagnosisinITER.This contributionprovidesacomprehensiveaccountonplasmaimpactondiagnosticmirrorsinJETwiththe ITER-LikeWall.SpecimensfromtheFirstMirrorTestandthelithium-beamdiagnostichavebeenstudied byspectrophotometry, ionbeamanalysis andelectronmicroscopy.Testmirrors madeofmolybdenum wereretrievedfrom themain chamberand thedivertorafter exposureto the2013–2014 experimen- talcampaign.Inthe mainchamber,onlymirrorslocatedattheentranceofthecarrierlostreflectivity (Bedeposition),whilethoselocateddeeperinthe carrierwereonlyslightlyaffected.Theperformance of mirrors inthe JET divertor was strongly degraded by deposition of beryllium,tungsten and other species. Mirrorsfrom thelithium-beamdiagnostichave beenstudied forthe firsttime.Gold coatings wereseverelydamagedbyintensearcing.Asaconsequence,materialmixingofthegoldlayerwiththe stainless steelsubstrateoccurred. Totalreflectivitydroppedfromover90% tolessthan60%,i.e.tothe leveltypicalforstainlesssteel.

© 2017ElsevierLtd.

ThisisanopenaccessarticleundertheCCBY-NC-NDlicense.

(http://creativecommons.org/licenses/by-nc-nd/4.0/)

1. Introduction

InITER,opticaldiagnosticswillrelyonmetallicmirrors,known as “first mirrors”, to access plasma while maintaining neutron shielding.Optical stabilityof firstmirrors willbe essential toen- surereliabilityofdiagnostics[1].Firstmirrors willundergomodi- ficationduetoplasma-wallinteraction(PWI)processes.Erosionby impingingparticleswillchangeroughnessandchemicalcomposi- tionofmaterial byco-implantation.Depositionofplasmaimpuri- tiestogetherwithfuelspecieswillleadtotheformationofcoating layersonthesurfaceofmirrors.Bothsituations willresultinthe degradationofreflectivity.There isan ongoing research infusion experimentstoassesstheperformanceoffirstmirrorsandtoelab- orate solutions to prolong their lifetime. Some examples are the worksatJET[2],TEXTOR[3],DIII-D[4],ToreSupra[5]andHL-2A [6].Also,laboratoryexperimentsonsimulationofneutron-induced

Corresponding author.

E-mail address: alvarogc@kth.se (A. Garcia-Carrasco).

1 See the Appendix of F. Romanelli et al., Proceedings of the 25th IAEA Fusion Energy Conference 2014, Saint Petersburg, Russia.

effectsarecarriedouttoassesstheimpactoftransmutation,mate- rialdamageandheliumproductiononopticalpropertiesofmirrors [7,8].

Theaimofthiscontributionistoprovideacomprehensiveac- counton themodificationofdiagnosticmirrors byPWIprocesses in JET with the ITER-Like Wall (ILW) [9]. Twodifferent types of mirrors have been studied: specimens fromthe First Mirror Test (FMT) [10-12] and, for the first time, mirrors from the lithium- beamdiagnostic.

TheFMTprojectisrealisedforITERwiththeaimtodetermine plasma impact on the optical performance ofdiagnostic mirrors.

The project started in 2001 on the request of the ITER Design Team. The FMT research program involves: (i) selection ofmate- rialformirrors,(ii)productionofmirrorsandtheircarriersforin- vesselinstallation,(iii)opticalpre-characterization,(iv)exposurein differentlocations inJET (main chamber anddivertor) duringan entireoperationalcampaign, and(v) comprehensivepost-mortem analyses by means of surface-sensitivetechniques to assessopti- calpropertiesandmorphology.Untilnow,completesetsofresults havebeenobtainedaftertwoexperimentalcampaignsinJET-C,i.e.

withcarbonwalls[10,11]andafterthefirstexperimentalcampaign http://dx.doi.org/10.1016/j.nme.2016.12.032

2352-1791/© 2017 Elsevier Ltd. This is an open access article under the CC BY-NC-ND license. ( http://creativecommons.org/licenses/by-nc-nd/4.0/ )

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Fig. 1. Top of the JET vessel: 1,2) beryllium limiters, 3) crane rail, 4) periscope head with Li-beam diagnostic mirror.

(2011–2012)inJET-ILW[12].Thisworkconcentratesonmirrorsex- posedduringthesecondILWcampaignin2013–2014.

Thepurposeofthelithium-beamdiagnosticsystematJETisto measureelectrondensityprofilesattheplasmaedge.Itisbasedon theinjectionofaneutrallithiumbeamwithenergiesof20–70kV andthesubsequentanalysisofphoton-emission profilesproduced bytheinteractionoflithiumwithplasmaelectrons.Becauseawide varietyofplasmashapesareexploredatJET,itisnecessarytouse amirror withan adjustabletiltangletodetectlight froma given region of interest at the plasma edge [13]. It should be stressed that theseare the first-evermaterial studieson actual diagnostic mirrorsfromJET.

2. Experimental 2.1. Mirrors

Twenty test mirrors were retrieved from JET-ILW after the 2013–2014experimentalcampaign.Allmirrorsweremadeofpoly- crystalline molybdenum with a surface area of 1× 1cm2. Some surfaceswereadditionallycoatedusingmagnetronsputteringwith a 1

μ

mthick layer ofmolybdenumorrhodium[14,15].Test mir-

rors were installed in stainless steel carriers placed in the outer mid-plane of the main chamber wall and in the divertor: outer andinnerlegandbelowthebasetile.Thecarriershadchannelsin which mirrorscould be mountedatdifferentdepths, thushaving differentsolidangleswithrespecttotheplasma.Theinformation aboutthecarriersandtheirinstallationintheJETvesselisdetailed in[2].

The Li-beamdiagnostic mirrorswere retrievedafterthe2011–

2012 and 2013–2014 experimental campaigns. The mirrors were 13× 5cm2 and1cmthickplatesmadeofbulkstainlesssteelwith a goldcoating.Theywereinstalled inaperiscope headontop of thevesselatabout42cmfromplasma.Fig.1showsthetopofJET vessel with the Li-beam diagnostic mirror in the periscope head surroundedbyvarioustypesoflimiters,e.g.castellatedmushroom roof limiters. Thelocation inthe JETvessel ofallstudied mirrors ismarkedinredinFig.2.

The total plasma exposure time during the 2013–2014 cam- paignwas19.5h(13.5hindivertorconfiguration)andthetotalen-

Fig. 2. Cross-section of JET. Test mirrors are located in the outer mid-plane and in the divertor area. The Li-beam diagnostic mirror is located in the top of the vessel.

(For interpretation of the references to colour in the text, the reader is referred to the web version of this article.)

Table 1

Comparison of parameters between the first (2011–2012) and second (2013–2014) campaigns at JET-ILW.

2011–2012 2013–2014 Total plasma time (h) 18.9 19.5 Divertor plasma time (h) 13.1 13.5

Input energy (GJ) 151 201

Injected D (10 23 atoms) 1165 1826 Injected N (10 23 atoms) 5 19

ergyinputwas201GJ.Theinjecteddeuteriumwas2× 1026atoms andtheinjectednitrogenasextrinsicradiatorwas2× 1024atoms.

Table 1 presents a comparison of parameters between the first andsecond ILWcampaigns. When comparing to ITER, the entire 2013–2014campaigncorrespondsintermsoftimeto122ITERdis- charges(400s,Q=10)butonlyto4ITERdischargesscaledbyen- ergyinputandabout1ITERdischargedintermsofdivertorfluence [16].

2.2.Analysismethods

Themostimportantpropertyofamirrorislightreflectance.To- talanddiffusereflectivityofmirrors wasmeasured inthevisible andnearinfra-redrange(400–1600nm).Surface andnear-surface composition of mirrors was examined using several complemen- taryaccelerator-basedmethodsattheTandemAcceleratorLabora- tory(Uppsala University,Sweden).Deuterium andberylliumcon- centrationsweremeasuredbynuclearreactionanalysis(NRA)with a 2.8MeV 3He+ beam. This method cannot be used to measure carbon in beryllium contaminated samples because protons pro- ducedfromthenuclearreactions12C(3He,p)4Heand9Be(3He,p)11B have similar energies and the resulting energy spectrum cannot be resolved. Tungsten concentration wasmeasured usingRuther- fordbackscattering spectrometry(RBS),alsowitha2.8MeV 3He+ beam.ThethicknessofthegoldcoatingoftheLi-beamdiagnostic mirrors wasmeasured by RBSusing a 3MeV protonbeam. Con- centrationoflightspecies(Be,C,NandO)wasmeasuredbytime- of-flightheavyionelasticrecoildetectionanalysis(ToF-ERDA)with a36MeV127I8+beam.Thismethodissuitedtodeterminecompo- sitiondepthprofilesbecauseofexcellentmassseparationbetween light elementsand good depth resolution of a few nm [17]. The maindisadvantageis thesensitivitytosurfaceroughnessbecause

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Fig. 3. Visual inspection of divertor mirrors after exposure to plasma.

Fig. 4. Reflectivity of outer divertor mirrors before and after exposure to plasma.

The distances 0.0, 1.5, 3.0 cm refer to the depth of the mirror in the channel of the carrier. The solid and dashed lines correspond to total and diffuse reflectivity respectively.

oflowincidenceangle (22°).However, thisisnot anissuein the analysisofmirrors.

The morphologyandcompositionofmirrorsurfaceswasstud- ied also by means of optical and scanning electron microscopy (SEM)usingHitachiSU8000(beam energy0.5–30keV) combined withenergy-dispersive X-rayspectroscopy(EDS ThermoScientific UltraDry,typeSDD– silicondriftdetector)andYAGBSE(backscat- teredelectrons)detector. TheEDSsystemis capableof beryllium detectionand quantification, as shown earlier in studies of dust specimensfromtheJETdivertor[18].

3. Results

3.1.Firstmirrortest

3.1.1. Mirrorsfromthedivertor

Visual inspection revealed that all divertor mirrors were cov- eredwithsmooth-lookinglayers displaying avariety of colourful patternsthus indicating inhomogeneous material deposition. The appearanceofseveralsurfacesispresentedinFig.3.The totalre- flectivitywasdegradedby50–80%regardlessofthesubstratema- terialor thelocation inthe carrier. The plotin Fig. 4shows the reflectivityfortheouter divertormirrors beforeandaftertheex- posuretoplasma.Thedistancesinthelegendrefertothedepthof themirrorinthechannelofthecarrier.Thesolidanddashedlines correspondtototalanddiffusereflectivityrespectively.Diffusere-

Fig. 5. Concentration depth profile of rhodium mirror located in the inner divertor, 1.5 cm deep into the channel of the carrier.

flectivitywasverysimilarforallmirrors(below5%)andonlyone traceisshowninthefigureasareference.

SurfacecompositionofdivertormirrorsispresentedinTable2. Themainimpurityisberyllium,followedbyoxygen,nitrogen,deu- terium,carbon,tungstenandtracesofInconelconstituents(Ni,Cr, Fe);thelatterisnotshowninthetable.Thetotalthicknessofde- posits is in the range from 50nm to 1μm. Such layer thickness completely blocks the light from reaching the mirror substrate.

Thisexplainswhyreflectivityofallmirrorsisdegradedtoasimilar levelregardlessofthepositionandthesubstrate(MoorRh).The reflected signal originates fromthe deposit itself. As a reference, the intensity oflight fallswhen penetrating Mo and Bewith an exponential decaylengthof13 and15nm respectivelyat600nm [19,20].

Impurity concentrations are similar to those measured on the mirrors exposed to the 2011–2012 experimental campaign [12] with the exception of carbon, whose levels are significantly lower,approximatelybyafactorof5.Themainreasonisthatdur- ingthe 2011–2012experimental campaign,mirrors were installed in-vessel right after changing fromthe carbon to the metal first wall.Duringtheinitialoperationphasein2011,carbonconcentra- tion in plasma wasdecreasing to values approximately 15 times smallerthanmeasuredinJETwithcarbonwallandthislowerlevel remained during the remaining part of the campaign [21]. That tendency was also perfectly reflected by HIERDA measurements on mirrors from the first ILW campaign [12]. It is also stressed that low carbon levels havebeen measured in2013–2014 opera- tion[22].Theincreaseduseofnitrogenasextrinsicradiatorinthe secondcampaignmighthavealsocontributedtothelowercarbon deposition bythe so-calledscavengingeffect[23].An exampleof concentrationdepthprofilesisshowninFig.5.Itisrecordedfora rhodium-coatedmirrorfromtheinner divertorplaced1.5cminto the channel ofthe carrier.Tracesforonly some impurity species (Be, O, C, N) are shown for clarity of the figure. The thickness

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Fig. 6. Reflectivity of main chamber mirrors before and after exposure to plasma.

The distances 0.0, 2.0, 3.0, 4.5 cm refer to the depth of the mirror in the channel of the carrier. The solid and dashed lines correspond to total and diffuse reflectivity respectively.

Table 3

Composition of deposits of main chamber mirrors.

The distances 0 cm and 1.5–4.5 cm indicate depth into the channel of the carrier. All numbers are in units of 10 15 cm −2 .

0 cm 1.5–4.5 cm

D 390 3–20

Be 7300 0–5

C 30 20–30

N 94 0–5

O 1125 1–20

W 2 0

ofthe depositisapproximately100nm. Itis composedmainlyof berylliumandoxygen.Theincreaseofoxygenatadepthof50nm is most probably associated with the in-vessel intervention (and venting the torus) to retrieve a broken reciprocating probe. The measuredfluctuationoftheoxygencontentindepositsreflectsthe machineoperationhistory.Onemaytentativelystatethattheoxy- gen detected in the co-deposit is associated with in-vessel pro- cesses (co-depositionofOimpurity species)andnot withtheox- idation of the entire layer once mirrors were removedfrom the torus.

3.1.2. Mirrorsfromthemainchamber

Thereflectivityplotsforthemirrorsfromthemainchamberare showninFig.6.Thesolidanddashedlinescorrespondtototaland diffusereflectivityrespectively.Diffusereflectivitywasverysimilar forallmirrors(below5%)andonlyonetraceisshowninthefigure asareference.Thereisadecreaseintotalreflectivitybyabout20%

forthe specimenlocated attheentrance ofthe carrier.However, totalreflectivityofallothermirrorsismaintainedorevenslightly increasedinthe visiblerangeasaresultoferosionof Mooxides byimpingingneutralparticles,asdiscussedinmoredetailin[12]. Surface composition of the mirrors is presented in Table 3. Thereisa significantdifferencebetweenthespecimenatthecar- rierentranceandthoselocateddeeper.Inthelattercasethecon- centrationsofD,Be,C,NandOimpuritiesareatthelevelofabout 1–3× 1016 cm−2, while tungsten is below the detection limit of 5× 1013cm−2. On the contrary, the mirror at the entrance (po- sition 0cm) is coatedby a layer of600nm composed mainly of beryllium. Photographic survey performed duringthe shut-down showedmeltingofberylliumlimitersinthevicinityofthemirror carrier.Thefairlythickberylliumlayerwasmostprobablyformed during such off-normalevents, including the damage to limiters

Fig. 7. Images of beryllium splashes on the surface of the mirror at position 0 cm.

The splashes have elongated (a-d) or flat (e) shapes. Images (a) and (b) show the same particle under electron and optical microscopy respectively.

(especiallyupperdumpplate)causedbyrun-awayelectronsinex- perimentsperformedattheveryendofthecampaign.

Results ofdetailed topographical studies performedwithSEM andEDSon themirroratposition 0cmare shownin Figs.7and 8. On top of the fairly uniform co-deposits there are numerous macroscopicparticlesofvariousshapeandsize:from3

μ

mtoover

100

μ

m.Theseare elongatedsplashes (Fig.7 (a–d)),flatsplashes

(Fig. 7(e)) and spherical droplets (Fig. 8(a)). The variety of ob- jectsgivesstrongindicationthat theywere depositedatdifferent events.Thesplashescannotbeassociatedwithasingledisruption becausetheyhavedifferentorientations.Acommonfeatureofall theseobjectsisthepresenceofberylliumasthemaincomponent.

Theotherdetectedelementsinallparticlesare:C,N,Oandtraces ofsteelandInconelalloyconstituents.Thesphericaldropletshown inFig.8(a)isnotsplashedanditscompositioniscomplex(seeEDS spectruminFig.8(b)).Besideslight elementstherearealsoheavy species:W,Mo,Ni,CuandFe.Thisgivesafairly strongindication that the originof such particle(s) is not associatedwith melting andsplashing ofthe limiter material. One maysuggest that it is mostprobablyaW-MoorW-Niparticleformedearlierinanother regionofthemachineandthentransported,forinstance,duringa disruption.

3.2.Li-beamdiagnosticmirrors

Li-beamdiagnosticmirrors wereretrievedafterthe2011–2012 and2013–2014campaigns.Imagesin Fig.9show the appearance ofthose mirrors. Inboth cases,significant areasof their surfaces weredamaged. Thetopography ofthedamagedarea, asrecorded byopticalmicroscopyinFig.10,clearlyproves meltingofthesur- facelayer(Au coatingandthestainlesssteelsubstrate)by arcing.

Arcingisa well-knownerosionprocess infusion devices[24-28]. The main conditions to formelectric arcs are a sufficiently high potential and an electron-emission spot such as a small surface protrusion (for instance, a beryllium droplet). In the presence of magneticfields,thecathodespotmovesacrossthematerialinthe directionperpendiculartothemagneticfield.Thiseffectisknown asretrograde motion and it produces characteristic dendrite-like tracks,asthoseobservedinthemirror[29].

Totalanddiffusereflectivityplotsinthevisibleandnearinfra- red range are presented in Fig. 11. The initial values were mea- sured on a spare twin mirror because the decision to study the mirrorwastakenafterplasmaexposuretodeterminethecauseof thedamageinthesurface.Totalreflectivitydecreasedafterplasma exposure from over 90% to about 60%. The values after plasma

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Fig. 8. (a) Spherical droplet on the surface of the mirror at position 0 cm, (b) EDS spectrum of the spherical droplet.

Fig. 9. Li-beam diagnostic mirrors after exposure in JET in a) 2011–2012 experi- mental campaign, b) 2013–2014 experimental campaign.

Fig. 10. Optical microscopy pictures of the surface of the Li-beam diagnostic mirror:

a) arc traces along the mirror surface, b) detail of material melting produced by arcing.

exposure resemble those characteristics for stainless steel. This suggests erosion of the gold layer and consequent mixing with stainless steel in the surface region. In the visible range, diffuse reflectivityincreasedfrom2%tomorethan15%asaresultofsur- facerougheningbyarcing.Inconclusion,optical propertiesofthe mirrorweresignificantlydegraded.

Fig. 11. Total and diffuse reflectivity of the Li-beam diagnostic mirror before and after exposure to plasma during the 2013–2014 campaign. (For interpretation of the references to colour in the text, the reader is referred to the web version of this article.)

The result of analysis with RBS for the mirror exposed dur- ing 2013–2014is presentedinFig. 12.Initially,there wasa well- definedgoldlayerof0.6

μ

m ontop ofastainless steelsubstrate.

After exposure, the gold signal is reducedand overlaps withthe stainless steelbackground. This indicates a reduction inthe gold concentration by a factor of 2 (from 3.7 to 1.8× 1018cm−2) and strongmaterial mixingbeingaresultofmelting.Inthe damaged area,theconcentrationsofDandBewereupto5× 1017cm−2 and 10× 1017cm−2,respectively.Theoriginoftheseimpuritiesisprob- ably splashing of the melt layer from nearby beryllium limiters (see Fig. 1). The splashed beryllium could act as a hot spot for theinitiationofelectricarcs.Theother possibilityforcreatingthe firstprotrusionwasalocaldetachmentoftheAucoating.Inaddi- tion,theimpactofso-called“parasiticplasma” duetolocalelectric fieldsintheperiscopesystemcannotbeexcluded,thoughitisdif- ficulttoprove;nodirectmeasurementcanbeperformed.Thecon- ceptofsuchdischargesinnarrowspaceswasproposed[30-32].In thenon-damagedarea,theconcentrationsofDandBeweremuch lower(about1× 1016cm−2)becauseoftheprotectiongivenbythe cranerailplacedinfrontoftheperiscopehead.

4. Concludingremarks

There are several importantcontributions ofthis work to the determination of plasma impact on the mirror performance and

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Fig. 12. RBS spectrum of the Li-beam diagnostic mirror before and after exposure to plasma during the 2013–2014 campaign.

on material erosion andtransport in the main vessel and inthe divertor.Studiesperformedwithasetofcomplementarymaterial analysistechniquesclearlyshowberylliumsplashesandfinemetal (W,Ni)dropletsdeposition onmirrorsurfacesinthemaincham- ber.ThishasneverbeenobservedatearlierstagesofFMT,neither in JET-C nor in JET-ILW. Mirrors in the divertor are coated with multi-layer deposits containing both W and Be [33], thus prov- ing transport of metalsto shadowed regions. Mirrors, with their smoothsurfacescanbeconsideredasperfectdepositionmonitors.

This type ofprobes withmirror-finish surfaces canserve in ITER aslong-termsamplestoassessmaterialmigration[34].UsingToF- ERDA depth profiling, one can then “deconvolute” the operation history.Itshouldbestressedthatall specimens,both inthemain chamber andinthedivertor, containednitrogenwhichwasorigi- nally puffedonlyin thedivertorregion. Nitrogenlevels are fairly constant overtheentireoperation period.Carboncontentinmir- rorsisabout5timeslowerinthesecondcampaignwithrespectto thefirst campaign.Detection ofonlytracesofcarbononsurfaces provides a positivemessage regardingthestabilityofW coatings ontilesmadeofcarbonfibrecomposites(CFC).

Degradationofreflectivitybydepositionofberylliumandother impuritiesonthemirrors exposedinthemainchamber hasbeen effectivelyreducedby placingthemirrorsdeeperinthechannels.

This experimental fact hashad an impact onthe ongoing design ofreactor diagnostics.Adedicatedmirror holderofhas beende- velopedintheITER– JET cooperationanditwasinstalledonthe mainchamber wallofJET[35].Inthedivertorarea,reflectivity of all mirrors hasbeensignificantly degraded regardlessofthe sub- stratematerialorthepositioninthechannel.InITER,thesituation willmightbeevenworseduetotheupscaleinmaterialmigration as a consequence of higher input energies and plasma exposure time.Theseresultshighlighttheneedoftechniquestomitigatere- flectivitydegradationofmirrors.Photonicmethodsareconsidered toremoveco-deposits.However,thisapproachrequiresbeforehand knowledgeofthecompositionandthicknessoftheco-depositsto setuplaserparametersinordertoavoidsurfacedamage.Photonic methodsweretestedonJETmirrorswithberyllium-containingde- posits and they did not provide satisfactory results [36-38]. The useofreplaceableprotectivefiltersisalsoruledout becausethey would be promptly degraded by gamma andneutron irradiation.

Methods basedonradio frequencyplasmageneratedlocallyclose to the mirrors are under development, but early results indicate the increase ofdiffusereflectivity ofthe cleanedsurfacesofmir- rorsfromJET [39]. Thebest resultssofar havebeenobtainedby mechanicalcleaning[40].Itshouldbestressedthatallabovemen- tionedworks[36-40] were carriedout ex-situ,i.e.onmirrors re- trievedfromJETandthencomprehensivelycharacterisedafterthe

exposure. Baffled channels with a series of fins are being tested toreduceimpuritydepositiononmirrors;resultsfromJET-ILWare stillunderevaluation.Othersolutionspointtotheuseofshutters tolimitplasmaexposuretime. Cassetteswithreplaceablemirrors arealsoconsideredforthedivertorregionwheredepositioneffects mayverystronglyreducethereliabilityofmeasurements.

Forthefirst time, surfaceanalyses havebeen performedona diagnosticmirror fromJET.Part ofthesurfaceofthe Li-beamdi- agnosticmirrorwasseverelydamagedbyintensearcing.Thegold coating layer andthe stainless steel substrate of the mirror had beenmelted,changingcompletelyitsopticalproperties.Themost probablyreasonfor arcinitiation issplashing of molten material fromthe surroundinglimiters. This ideais supported by thesig- nificantlyhigheramountofdepositsfoundinthearea affectedby arcingwithrespecttothenon-damagedarea,whichwasprotected fromimpurity deposition byacrane railstructureplaced infront oftheperiscopehead.

Theseresults contribute to the discussion on theapplicability ofcoatedmirrorsandtheyalsostronglypointtotheneedofvery careful selection of mirrors locations, including the surrounding, andthedesignofdiagnosticchannels.Theongoingtestoftheded- icatedmirrorholderinthemainchamber[35]isexpectedtopro- vide further indications for the design process. In summary, the studies of mirrors have had an impact on the development and testingofseveralschemesfortheprolongationofmirrors’lifetime, i.e.cleaningandprotection.

Acknowledgements

This work has been carried out within the framework of the EUROfusion Consortium and has received funding from the Eu- ratom research and training programme 2014–2018 under grant agreement No 633053. The views and opinionsexpressed herein donotnecessarilyreflectthose oftheEuropeanCommission.The workhasbeenpartlyfundedbytheSwedishResearchCouncil(VR) through contracts no.621-2012-4148 and 2015-04844. We thank thestaff oftheTandemAcceleratorLaboratoryattheUppsalaUni- versityfortheirhelpduringtheionbeamanalysismeasurements.

TheauthorswouldliketothankHéctorEscorialforhishelpinthe processingofopticalmicroscopyimages.

Supplementarymaterials

Supplementary material associated with this article can be found,intheonlineversion,atdoi:10.1016/j.nme.2016.12.032.

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