Analysis of water samples saved during 1939-40 campaign by Great Lakes Company

(1)

COpiea

te:

ANALYSIS OF WATER SAMPLES SAVED DURING

1939-&0 CAMPAIGN

LONGMONT lACmRY

'l'RE

GREAT WESTERN SUGAR COMPANY

GGD.eral SUper1n.ten-deat

-==-Geueral Chemiat

District Engineer

SUpel"1ntendent

Ohiet Clumuat

ffeJ~

Chiet Chem.tat

MV

'1

₁

1940

~'\

y

....

GEN'L

,

~

19 iO

G,

w '"'

_{. "• co}

.,..,,

(2)

INDEX

'l'O

WATI!E

ANALYSIS

K,iJ:ld

ot

.

Wat•~~~

_l!!e.,...NO,

Boue,.- J'eed

1 PNes Woll

2 :eatt•rr su.pply

3 Whit& Oenlrit'ugel.

Wull

• Water

tn

Br;ril••

i

Cit,-

water

6 B1'Nr

Wate

(3)

Form 443-2M-7-34-Pads 100

WATER ANALYSIS

I

... LollglllPU

~

....

..

:

...

.

..

...

.

...

Factory

.

..

.

...

-

_&'3 ... '/

L-

i

ffQ_ __

···-··-···-···.193

Kind of Water:

Boiler :reed

Description of Sample:

Compoaite aemple taJctn

c1U1"1ng

eampai

Sampled about

on.oe

a week.

1939-40

Source of Water:

Dripa

trom

at.am ollamber•

ot

2nd.,3rd,.&th,

etfMta

ot the eTapo:ratora, Dr1pa

trm

the pen ooil•, steea

trapa

tram

ell

aain atea

lin••

and oocuion.ell7

Silica Iron Calcium Magnesium Sodium Chlorine Sulphuric Acid Carbonic Acid

l

e

t. body- eftp. and 5th. bod7

eTap. dripa.

ANALYSIS Parts Per 100,000 SiO, Fe Ca Mg Na Cl so, co. HYPOTHETICAL COMBINATIONS Silica s10.

Sodium Chloride NaCl Sodium Sulphate Na,SO, Sodium Carbonate Na.co. Magnesium Chloride MgC11

Magnesium Sulphate MgSO, Magnesium Carbonate MgC01 Calcium Chloride Calcium Sulphate Calcium Carbonate Ferrous Carbonate CaC11 CaSO, caco, FeCO,

Organic and Volatile (by difference)

TOTAL SOLIDS

.eo

Organic and Volatile (by difference) TOT·AL SOLIDS

COPIES TO

_parts

_{per million on}

_original.

_water

~

1')81'ta per million

on

original. water

ree

22.1,

Total

22.u.

Parts Per 100,000

2.eo

General Supt. General Chemist Asst. General Supt. District Engineer Superintendent Laboratory

There aeans

be

no

combined

en t.

rr

.

..L

-···-·-···--pre a

Ltl1'._:J_~c.;;,,c;;;...,,.,.

--····

(4)

Form 443-2M-7-34-Pads 100

WATER ANALYSIS

... Lonpont ...

Factory

... _ay ...

'1

_. ___

l

~40 •

...

193

Kind of Water:

Presa

Wash

_{Composite amnple teken during}

_campaign

₁₉₃₉

Sampled

about

on.ee

a

week.

source of Water:

Drips

from

lat. etteet

ot

the eTaporatora, drips from the following

heater•:

thin

juice, raw juioe,

2nd.

Pr•••,

gentera,

battery heaters,

alao

blow-up

t,apa,

and over-flow from Boiler teed tank, Also

eom,

city' water to

lower

the temperature.

ANALYSIS Silica SiO, Iron Ire Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulphuric Acid so,

Carbonic Acid co.

Organic and Volatile (by difference) TOTAL SOLIDS COPIES TO Parts Per 100,000

2.20

HYPOTHETICAL COMBINATIONS Silica s10.

Sodium Chloride NaCl

Sodium Sulphate Na,SO,

Sodium Carbonate Na.co.

Magnesium Chloride MgCl.

Magnesium Sulphate MgSO,

Magnesium Carbonate MgC01

Calcium Chloride CaCl.

Calcium Sulphate CaSO,

Calcium Carbonate ea.co,

Ferrous Carbonate Feeo.

TOTAL SOLIDS

Parts Per 100,000

2.20 ~

/

~

f'r

~

.

L

-···----·-·-r::?.\?

__ .:

..

0. ...

~ c h e m l s t . --····-·-····""-··-·

(5)

Form 443-2M-7-34-Pada 100

WATER ANALYSIS

... Longmont···-···Factory

.... ~ay ..

~

• ...

lMO

·--···-··-···--

· ···-···.193

Kind of Water:

Bil'Uerr Supply

CClllpo811:

•ple

tak,

4ur1Dg

the

csnpai,

1939-40

Seapled about onoe a nek.

source of Water:

Condeued

water

trcm

the North J'ront

ETajlorator

Condenaer(

city water on

leg)

Con.denaed water

hoa

oliTer nouum ayatem ( city water

on leg)

Cooling water

tl'Oll

gaa

pUlllpa, Dl"tpa

troa

batterr

oalorizatora, OTertlow

from preae

wan

tank,

and

ocoaaionally water t'rom pan

oondenaer

aeal

tank,

alllO

water fl'om Th1ok

Jui••

heater drip• and granulator eoila.

'

ANALYSIS Silica Si01 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulphuric Acid so.

Carbonic Acid co.

Organic and Volatile (by difference) TOTAL SOLIDS COPIES TO

General Supt. General Chemist Asst. General Supt. District Engineer Superintendent Laboratory Parts Per 100,000

rs.oo

( 3 )

HYPOTHETICAL COMBINATIONS Silica s10.

Sodium Chloride NaCl Sodium Sulphate Na.so, Sodium Carbonate Na.co. Magnesium Chloride MgC11

Magnesium Sulphate MgSO, Magnesium Carbonate Mg001 Calcium Chloride Calcium Sulphate Calcium Carbonate Ferrous Carbonate CaCI1 CaSO, CaCO, Feco.

Organic and Volatile (by difference) TOTAL SOLIDS

Parts Per 100,000

5.00

(6)

Form 443-2M-7-34-Pads 100

WATER ANALYSIS

... L~~glllOJl

t ..

.

...

.

...

.

...

.

....

..

...

.

..

....

.

Factory

Kind of Water:

White centr

i

fugal

waah water

Com

pos

i

'Ce sample

t

o

r the

oampa

i

Samp

l

ed about once a

week

.

.. May .

.

'1

., ...

.

19 4:0

.• -

·

· ···

··

····

· -

···

·

· -·

··

···

· .193

1 9S....40

Source of Water:

_{Condensed wator}

_trom

_3rd

_.

_{ettect evaporato?'}

_,

_{usually- from the N}

_o

_rth

_a

_i

_de

_.

ANALYSIS Silica Si01 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulphuric Acid so.

Carbonic Acid co.

Organic and Volatile (by difference) TOTAL SOLIDS COPIES TO 1

General Supt. General Chemist Asst. G«;tllel'.3.1 Supt. District Engineer Supe!yihtend ent Laboratory I

I

Parts Per 100,000

1 .

20

HYPOTHETICAL OOMBINATIONS Silica s10.

Magnesium Chloride MgC11

Magnesium Carbonate MgC'O,

Calcium Chloride cam.

Calcium Sulphate caso.

CJalcium carbonate caco.

Ferrous Carbonate Feco.

Parts Per 100,000

1 .

20 ---·

-

··-··

/01

:

__

p~--·

Chlet Chemist.

· ··

-·-

·

(7)

Form 443-2M-7-34-Pads 100

WATER ANALYSIS

LO~Ollt

...

Factory

···-···-··· ... ----

.. 1481'

..

7 •....

~

9~·--·-···-···-···-···.193

Kind of Water: Description of Sample: Source of Water:

Water

in

ilere.

Com.poeite sample

or

water taken trom

all

boilers during 1939-4.0

Campaign

Sm:i:ples token about once a week,atter

tbe

t1rat

no

weeka

ot

oempaign,

For

thi•

reason and beoauae sanewhate larger average samples were taken

later in the campaign in order

to

have suttic1ent water '!or analysis,

The

total

solid• show hip.her tor the eanPQsi te aanple than doea the

weekly

average

shown ou. ihe oapaign sheets.

J'rom

all Boiler• in aef'fioe.

Campaign. Sheet Averages

1950 lba. Soda

A.ah

(

38.2 lbs.

per

Day)

Alkalinity

.o-

.

Hardness

o.•

•5

ft

cauatio

sotrcL( o.g

ft ft • )

Solids

18'.

600

ft

S0d1um. Phosphate (

11.a lba.

per Day)

Campaign

OODlposi

te

ample

ot boiler water Phenolphthalein Alkalini t7

.002

Hardneaa

by

aoap,

o.50

cafouiatecr

Hardn•t

-

,

ot

water

1n

boilers

o.7~

ANALYSIS HYPOTHETICAL COMBINATIONS

Silica SiO, Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulphuric Acid so,

Carbonic Acid co.

"

Phosphate

_PO.fa

Organic and Volatile (by ditterence) TOTAL SOLIDS Parts Per ~000

2.30 .3l

.'3

.oa

50.80

1.33

13.02

57.87 .35

l2S.49

102.01

228.50

Silica SiO,

SOdium Pho~hate N~ PO,

Magnesium C oride Mg •

Magnesium Carbonate Mg008

Calcium Chloride CaC11

calcium Carbonate eaco.

COPIES TO _~

_{Parta per million on original}

_water

NI¼ " "

"

Parts Per 100,000

2.30

2.19

19.25 l00.16

.60

.28

1.07 .M

126.4:i

102.01

228.50

General Supt. General Chemist Asst. General Supt. District Engineer Superintendent Laboratory ~

P.P.

100,000

on

evaporated rea1due

Free

o.oo

Total 1.02

o.oo

---·-·-·-···~.

~~

..

:._ ..

1!~·-

Chtef Chemist.

-·--( 8

)

(8)

Form 443-2M-7-34-Pads 100

WATER ANALYSIS

Longmont

---·--·-···---···-···Factory

····--···-···

_{_May}

_{.. '··-··}

_{l 940}

_{·-···---···-···}

_·

_···.193

Kind of Water:

City

water

Composite sample taken dut1.ng the campaign 19Z9-40

Sampled about once a week.

Source of Water:

St. Vrain River about

15 mil•• weat

ot

Longmont

ANALYSIS Silica Sio. Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlm;ine Cl

Sulphuric Acid so.

Carbonic Acid co.

Organic and Volatile (by difference) TOTAL SOLIDS COPIES TO Parts~OOO

2.00 .oa

.51

.22

.11

.05

.16

1.52 .65

.80

5.

HYPOTHETICAL COMBINATIONS Silica sio.

Sodium Sulphate Na.so,

Sodium Carbonate Na,,CO,

Magnesium Chloride MgCl1

Magnesium Sulphate MgS.0,

Magnesium Carbonate MgOO,

Calcium Chloride CaCI1

Calcium Sulphate ca.so.

Calcium Carbonate eaco.

Ferrous Carbonate FeCO,

Organic and Volatile (by difference) TOTAL SOLIDS Parts Per 100,000

2.20 .os

.12

.15

.6

1.27 .l'l

4..65

.so

5.45 -··-···-·-···/i:6

' ...

f ~

Chief Chemist.

·--.

"

"-,,

(9)

Form 443-2M-7-34-Pads 100 ·

WATER ANALYSIS

...

.

...

LOJl4!Jll0:D.t

...

.

...

.

..

...

Factory

_..

...•...•...

_,y

_'1

1

····--···--

₁₉₄₀

··-

-

_··-·

_·

_{··-·-···-}

₁₉₃

Kind of Water:

River

Water

_Composite

_{eample ~aken during the campaign 19:ll}

_-40

Sampled about

once

a week.

Source of Water:

St

.

Vrain

r1Ter just South

of

the J'e.ctoey Site, Mostly Seepage Water

.

ANALYSIS Silica

s10.

Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulphuric Acid

_so.

Carbonic Acid

_co.

TOTAL SOLIDS COPIES TO

General Supt. General Chemist Asst. General Supt. District Engineer Superintendent Laboratory I It