Analysis of water for campaign 1946-1947 Billings factory

(1)

ANALYSIS OF

WATERS

FOR CAMPAIGN

1946-1947

BILLINGS FAC'IDRY

THE GREAT

WESTERN

SUGAR COMPANY

cc-

General

Chemist

~

Asst. Gen.

Supt.

Superintendent

District En

g

ineer

Laboratory

(2)

• INDEX

KI

N

D OF

W

ATER

PAGE

M

ain Tank

1 City

2

B

attery Supply

3

Press

W

ash

4

Centrifu

g

al

W

ash

5

Cold Saccharate

C

ake Wash

6

Boiler Feed

7

(3)

Form 443-2M-7-43- Pads 100

WATER ANALYSIS

...

.

..

.

...

Billings

...

Factory

.

....

.

....

.

..

May-_22

, ...

1947

...

194 ...

.

Kind of -Water:

River Water

Description of Sample:

Average

Sample for the

1946-47

Camap

'

i

g

n

Source of Water:

Y

el

low

stone

R

iver

Intake

_

one

mile

south of

factory

ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulfuric Acid _S04 Carbonic Acid C03 Phosphoric Acid _P04

Organic and Volatile (by difference)

TOTAL SOLIDS AT 105° C

COPIES TO

General Chemist Asst. General Supt. District Engineer Superintendent Laboratory Parts Per 100,000

1.76 .14

3 .

93

1.49

2 .

86 .82

9 .

09

7 .

07

27.16

56

27 .

72

HYPOTHETICAL COMBINATIONS Silica _Si02

Sodium Chloride NaCl Sodium Sulfate Na₂S04 Sodium Carbonate Na₂_C03 Sodium Phosphate _Na3P04 Magnesium Chloride MgC1₂ Magnesium Sulfate _MgS04 Magnesium Carbonate MgC03 Magnesium Phosphate Mg3(P04)2

Calcium Sulfate _CaS04

Calcium Carbonate _CaC03 Calcium Phosphate Ca₃_(P04)₂ Ferrous Carbonate _FeC03 Ferrous Phosphate Fe₃_(P04)z

1

-Parts Per 100,000

1 .7

6

1.35

7 .

20

5.29

1.46

9.81

•

29

27 .

16 ,

56

27 .

72

Chief Chemist.

(4)

Form 44S-2M-7·43-Pa,ds 100

WATER ANALYSIS

...

.

..

.

Billings

...

..

Factory

..

....

~~~¥.

..

?.~, ..

.

~.~.~?. .

....

..

...

194 ...

.. .

Kind of Water:

City

Water

.Average Sample

for the 1946-47

Camapaign

Source of Water:

River

water treated and filtered thru the

City

Wa

ter

Plant

ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulfuric Acid _S04 Carbonic Acid 003. Phosphoric Acid _P04

COPIES TO

1.28 .14

4 .

56

1 .

61

3 .

48 .

91

9 .

46

8 .

81

30 .

25

1.25

31.50

HYPOTHETICAL COMBINATIONS Silica Si02

Sodium Chloride NaCl Sodium Sulfate Na₂S0₄ Sodium Carbonate _Na2C0₃ Sodium Phosphate Na₃P0₄ Magnesium Chloride MgC1₂ Magnesium Sulfate MgS0₄ Magnesium Carbonate MgC0₃ Magnesium Phosphate Mg3(P04)2

Calcium. Sulfate CaS0₄

.Calcium Carbonate CaC0₃ Calcium Phosphate Ca₃(P0₄)₂ Ferrous Carbonate FeC0₃ Ferrous Phosphate Fe₃_(P04)₂

TOTAL SOLIDS AT 105° C - 2 -Parts Per 100,000

1.28

1.50

8 .

93

4 .

29

2 .

57

11.39 .

i9

30 .

25 J

·

25

31 .

50

Chief Chemist.

(5)

Form 448-2M-7-48- Parls 100

WATER ANALYSIS

Billings

...

Factory

..

....

.

...

May

.. 23,

..

1947 ...

194 ...

.

Kind of Water: Description of Sample: Source of Water: ANALYSIS Silica _Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulfuric Acid _S04 Carbonic Acid C03 Phosphoric Acid _P04

Battery Supply

Average Sample for the 1946-47 Camapaign

All drips from hot

condensors

of ev.aporators,

drips from Vapor Pan

,

overflow from press wash

Parts Per 100,000

1.36 .

10

3 .1

3

1.24

2.35 .71

6.87

6.03

21.79

1.45

HYPOTHETICAL COMBINATIONS Silica _Si02

Sodium Chloride NaCl Sodium Sulfate Na₂_S04 Sodium Carbonate _Na2C03 Sodium Phos,phate Na₃_P04 Magnesium Chloride MgC12

Magnesium Sulfate _MgS04 Magnesium Carbonate MgC03 Magnesium Phosphate Mg3(P04)2 Calcium Sulfate _CaS04 Calcium Carbonate _CaC03

Calcium Phosphate _Ca3(P04)2

Ferrous Carbonate FeC0₃ Ferrous Phosphate _Fe3(P04)2

23 .

24

COPIES TO

General Chemist Asst. General Supt. District Engineer Superintendent Laboratory - 3 -Parts Per 100,000

1.36

1.17

5.84

3.66

1.73

7.82

•

21

21.79 l.4.5

23. 24

Chlet Chemist.

(6)

Form 448-2M-7-48-Pads 100

WATER ANALYSIS

Billings Factory

...

.

..

.

....

...

.

..

...

.

...

.

...

.

.... Factory

...

.

..

May

._

23 ,

_._1947 ..

.

..

...

..

...

....

..

194 ..

.

..

.

Kind of Water: Description of Sample: Source of Water:

Press Wash

Average

~ample for the 1946

-

47 Camapaign

Condensed

waters from

all

1st

effect

evaporators

,

Battery

Calorisators,

all heaters and overflow from

Boiler

Feed

.

Possible to send

Battery

Supply to Press

Wash,

and drips

from

all evaporators

,

blow up traps

,

and office heating

system.

ANALYSIS HYPOTHETICAL COMBINATIONS

Silica Iron Calcium Magnesium Sodium Chlorine Sulfuric Acid Carbonic Acid Phosphoric Acid Si02 Fe Ca Mg Na Cl S04 C0₃ P0₄

COPIES TO

l

.

7

Silica Sodium Chloride &odium Sulfate Sodium Carbonate Sodium Phos,phate Magnesium Chloride Magnesium Sulfate Magnesium Carbonate Magnesium Phosphate Calcium Sulfate Calcium Carbonate Calcium Phosphate Ferrous Carbonate Ferrous Phosphate Si0₂ NaCl Na2S04 Na₂C0₃ Na3P04 MgC12 Mg_S04 MgC0₃ Mg3(P04)2 CaS0₄ CaC0₃ Ca₃(P04)2 FeCO~ Fe₃(P04 )2

4

-Parts Per 100,000

1.7

(7)

Form 443-2M-7-48- Pe,ds 100

WATER ANALYSIS

···

··

···

·

· ···

··

·

· Billings .

... Factory

... May .. 23, __

1,947 ....

.

..

....

..

...

194 ..

...

.

Kind of Water:

Water

used to wash

white

sugar

Average

sample for the 1946-47

Cam:p:pign

Drips from the steam chest of the 3rd effect

of north evaporators

ANALYSIS HYPOTHETICAL COMBINATIONS

Silica Iron Calcium Magnesium Sodium Chlorine Sulfuric Acid Carbonic Acid Phosphoric Acid Si0₂ Fe Ca Mg Na Cl S0₄ C03 P04

COPIES TO

1.1

5 Silica Sodium Chloride Sodium Sulfate Sodium Carbonate Sodium Phosphate Magnesium Chloride Magnesium Sulfate Magnesium Carbonate Magnesium Phosphate Calcium Sulfate Calcium Carbonate Calcium Phosphate Ferrous Carbonate · Ferrous Phosphate Si0₂ NaCl Na2S04 Na₂C0₃ Na₃P0₄ MgC1₂ MgS04 MgC03 Mga(P04)2 CaS0₄ CaC03 Ca₃(P0₄)₂ FeC0₃ Fe₃(P0₄)₂

Parts Per 100,000

1.

1

(8)

Form 443- 2M-7-43- Pa..<ls 100

WATER ANALYSIS

Billings

...

.

... Factory

...

Ma

...

y 23

..

.

,

..

.

..

1947

..

...

... , ..

.

....

.

...

..

...

.

...

.

194 .

.

..

.

Kind of Water: Description of Sample: Source of Water: ANALYSIS Silica Si0₂ Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulfuric Acid _S04 Carbonic Acid C03 Phosphoric Acid _P04

Cold

Saccharate

C

ake

W

ash

W

ater

Average Sample

for the 1946-47 Camapaign

/

City water was

used 2/3rds of

G8II!Rign

W

ell

Water

of 80 parts p.p

.

100 ,

000 was

used l/3rd of

Cam.apaign

Parts.Per 100,000

1.96 .

17

5 .

12

2.

25

7.

22

1.32

17 .

69

10 .

64

46 .

37

1.77

HYPOTHETICAL COMBINATIONS Silica Si0₂

Sodium Chloride NaCl Sodium Sulfate Na₂S0₄ Sodium Carbonate Na₂C0₃ Sodium Phos,phate Na₃_P04 Magnesium Chloride MgC1₂ Magnesium Sulfate Mg_S04

Magnesium Carbonate Mg_C03

Magnesium Phosphate Mg3(P04)2

Calcium Sulfate C_aS04

Calcium Carbonate CaC0₃ Calcium Phosphate Ca₃(P0₄)₂ Ferrous Carbonate FeC0₃ Ferrous Phosphate Fe₃_(P04)₂

Parts Per 100,000

1.96

2 .

18

19 .

64

5.

53

3 .

92

3:;3Tljl9

12 .

79

•

35 ₄₈

_.

₁₄

46 .

37

J ,

77

48 .

14

COPIES TO

General Chemist Asst. General Supt. District Engineer Superintendent

Laboratory - 6

(9)

Form 443- 2M-7-4S-Pa,!s 100

WATER ANALYSIS

..

.

...

.

..

.

Billings .

..

.

..

.

..

.

...

.

.. Factory

.

...

.

..

May

.

.2

.

3 , .

.. l.9:4.'Z

.

...

.

..

.

.. 194 .

.

...

.

Kind of Water:

_Water

_in

_{Boiler Feed Tank}

_Average

_{sample for the 1946-47 Campaign}

Drips from

the

2nd

,

3rd

,

4th,

&

5th

bodies of the evaporators.

Drips

from pans after flashing to Exhaust

.

All live steam tr~ps

Silica Iron Calcium Magnesium Sodium Chlorine Sulfuric Acid Carbonic Acid Phosphoric Acid ANALYSIS Si0₂ Fe Ca Mg Na CI S0₄ C03 P0₄

COPIES TO

General Chemist Asst. General· Supt.

District Engineer Superintendent Laboratory Parts Per 100,000

2 .

2

- 7 ~ HYPOTHETICAL COMBINATIONS Silica Sodium Chloride Sodium Sulfate Sodium Carbonate Sodium Phos,phate Magnesium Chloride Magnesium Sulfate Magnesium Carbonate Magnesium Phosphate Calcium Sulfate Calcium Carbonate Calcium Phosphate Ferrous Carbonate Ferrous Phosphate Si02 NaCl Na2S04 Na2C03 Na₃P0₄ MgC1₂ MgS0₄ MgC0₃ Mg3(P04)2 CaS0₄ CaC0₃ Ca₃(P0₄)₂ FeC0₃ Fe₃(P0₄)₂

Parts Per 100,000 ,,

2.2

(10)

Form 443-2M-7-48- Pitds 100 • '

11 1 4.

WATER ANALYSIS

Billings

F

..

.

...

.

actory

...

Ma.y.

_

23,

__

1947 ...

... 194 ... .

Kind of Water:

_Water

_in

_Boilers

_Average

_{Samaple for the 1946-47 Camapaign}

Added

to

Boilers:

Source of Water: Silica Iron Calcium Magnesium Sodium Chlorine Sulfuric Acid Carbonic Acid Phosphoric Acid Si02 Fe Ca Mg Na Cl S04 C03 P0₄ ANALYSIS

COPIES TO

General Chemist Asst. General Supt!

District Engineer Supe;rintendent Labor.atory

\

]

'

or

Campaign

2650

1755

450 Per

Day

33.5

22.2

5.7 Caustic

Soda

Tr

i.Sod.

Phos

Sod. Sulphite

Alkalinity

Hardness

P04 ppm

Parts Per 100,000

.90

.14

.03

.05

37.77

1.22

11.89

38.24

6.00

96.24

8 6,36

182.60

- 8

-.016

.3

60

HYPOTHETICAL COMBINATIONS

smca

Sodium Chloride Sodium Sulfate Sodium Carbonate So,p.ium Phos,phate Magnesium Chloride Magnesium Sulfate Magnesium Carbonate Magnesium Phosphate Calcium Sulfate Calcium Carbonate Calcium Phosphate Ferrous Carbonate Ferrous Phosphate Si02 NaCl Na2S04 Na2C03 Na₃P0₄ MgC1₂ MgS04 MgC03 Mg3(P04)2 CaS04 CaC03 Ca₃(P0_{4 ) 2} FeC03 Fe₃(P0_{4 ) 2}