Analysis of waters for campaign 1950-1951 Billings factory

(1)

cc:

ANALYSIS OF

WATERS

FOR CAMPAIGN

1950-1951

BIIJ,INGS

FACTORY

THE GREAT

WESTERN

SUGAR COMPANY

General Chemist~

Asst.

Genl.

Supt.

Superintendent

District

Engineer

Laboratory

(2)

INDEX

KIND OF

WATER

PAGE

Main

Tank (River

Water)

1 City

2 Well

(Cold Saccharate

Wash Water)

3 Battery Supply

4 Press

Wash

5 Centrifugal

Wash

6 Boiler Feed

7

(3)

Form 443- 2M- 8-48-Pads 100

WATER

.

ANALYSIS

...

.

...

..

. Billings

....

.

...

Factory

.

...

!rnrtJ ...

~3..,

... l9.5.J

...

I9 ... .

Kind of Water:

_{River Wate}

_r

Description of Sample:

_{Average Sample for}

_{Campaign 1950-51}

8.1

pH

Source of Water:

Yell

owstone

River

Intake one

mile

south of factory

ANALYSIS HYPOTHETICAL COMBINATIONS

Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulfuric Acid

so.

Carbonic Acid

co.

Phosphoric Acid PO,

Organic and Volatile (by difference)

TOTAL DISSOLVED SOLIDS AT 105° C

COPIES TO

General Chemist Asst. General Supt. District Engineer Superintendent Laboratory

pH

Parts Per Million

18.6 L7

46.0

20.0

51.8

8 .

8

138.7

93 .

6

379.2 HLL1

397 .

6

Silica Si02

Sodium Chloride NaCl

Sodium Sulfate Na,SO,

Sodium Carbonate· Na2COa

Sodium Phosphate Na.PO,

Magnesium Chloride MgCl2

Magnesium Sulfate MgSO,

Magnesium Carbonate MgCOs

Magnesium Phosphate Mgs(P0,)2

Calcium Sulfate CaSO,

Calcium Carbonate CaCOa

Calcium Phosphate Caa(P0,)2

Ferrous Carbonate FeCOa

Ferrous Phosphate Fea(P0,)2

---

-1-Parts Per Million

18 .

6

14.5

142.4

53.1

32.2

114.9

379.2 ]

$

,

I,

397.

6

Chief Chemist.

(4)

Form 443-2M-8-48-Pads 100

...

J?.:JJ~J~P:g.1? ...

Factory Kind of Water: Description of Sample: Source of Water: ANALYSIS Silica SiO, Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulfuric Acid

so,

Carbonic Acid

co.

Phosphoric Acid PO,

COPIES TO

General Chemist

Asst. General Supt. District Engineer

pH

WATER ANALYSIS

...

Apr

.i

l

..

.23.,.

.

195.1 ...

19 ... .

City

Water

Averag

e

Sample

for

Campaign 1950

-51

pH

8 .1

R

iver

water

treated and filtered

by

City

W

ater

Plant

Parts Per Million

16.4

1.4

40 .0

12.9

27.4

7.9 8604

68.6

261.0

5.1

HYPOTHETICAL COMBINATIONS Silica Si02

Sodium Carbonate Na,COs

Sodium Phosphate NaaPO, Magnesium Chloride MgCI.

Magnesium Phosphate Mg,(PO,),

Calcium Carbonate CaCOs

Calcium Phosphate Caa(PO,), Ferrous Carbonate FeCOo Ferrous Phosphate Fe,(PO,),

Parts Per Million

16.4

13.0

68.9

49.9

9.7

99.9

261.0 5 ,]

266.1

(5)

Form 443-2M-8-48 -Pads 100

WATER ANALYSIS

Billings

---·--·-·--·--·----·-··-··---Factory _______________________________

April 23, 1951

____________________________________ 19 _________ _ Kind of Water: Description of Sample: Source of Water: Silica Si02 Iron Fe Galcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulfuric Acid

so,

Carbonic Acid

co.

Phosphoric Acid PO,

W

ell

W

ater (Us

ed

for Cold Saccharate

W

ash)

A

verage Sample for Campaign 1950-51

pH

8 .1

,

W

ell located south and adjacent to limestone ho

p

per

Parts Per Million

39.4

Silica Si02

2.1

47.2 ~2.4

Sodium Carbonate Na,COa

130.4

Sodium Phosphate Na,PO,

16.2

297.5

123.6

Magnesium Phosphate Mga(P0,)2

Calcium Phosphate Caa(PO,).

6

88 .8

l

6

COPIES TO

General Chemist Asst. General Supt, District Engineer Superintendent Laboratory

pH

-3-Parts Per MIiiion

39.4

26.7

370.3

59.0

71.1

690.4

Chief Chemist.

(6)

Form 443- 2M-8-48- Pads 100

WATER ANALYSIS

Billings

... Factory

...

..

...

.

...

AP.;r

.

:U

.

.. 23

.

;J

..

.1951.

..

.

...

19 ... . Kind of Water: Description of Sample: Source of Water: ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulfuric Acid

so,

Carbonic Acid

co.

Phosphoric Acid PO,

Battery Supply

Average ~ample for Campaign

1950-51

pH

7.6 All drips from hot condensors of

E

vaporators,

d

rips from vapor pan, overflow from press wash

HYPOTHETICAL COMBINATIONS

14.4

Silica Si02

1.0

21.6

Sodium Sulfate Na.SO,

12.4

Sodium Carbonate Na.COa

29.7

Sodium Phosphate NaaPO,

5.4

Magnesium Chloride MgCl,

86.8

44.0

Magnesium Carbonate MgCOa

Ferrous Phosphate Fes(PO,),

Organic and Volatile (by difference) TOTAL DISSOLVED SOLIDS AT 105° C

235.6

COPIES TO

General Chemist Asst. General Supt. District Engineer

pH

53.9

2.1

215.3 20,3

23506

(7)

Form 443 -2M-8-48- Pads 100

WATER ANALYSIS

.

...

..

.

..

.

....

.

....

.

..

Billings

....

.

..

.

....

Factory ...

Apr.il

...

23..,.

.

.19Sl

..

.

..

.

...

.

....

19 ... .

Kind of Water:

Press

W

a.§h

Average

Sample

for Campaign 1950-51

Source of Water: ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulfuric Acid

so.

Carbonic Acid

co.

Phosphoric Acid PO,

COPIES TO

General Chemist Asst. General Supt. District Engineer Superintendent Laboratory pH c;

p

H

9.1 Condensed waters from all 1st effect evaporators, battery

calorisators,

all heaters

an

d

overflow from Boiler Feed.

Possible

to

send battery supply to press wash,

and

d

rips

f

ro

m

all evaporators and

b

low-

up tr

aps

Parts Per Million Parts Per Million

39

0

9 .1

-5-Silica Si02

Sodium Carbonate Na,COs

Magnesium Chloride MgCl,

Magnesium Phosphate Mgs(PO,),

Calcium Phosphate Cas(PO,).

Ferrous Phosphate Fea(PO,).

3

9.0

9 .1

(8)

Form 443- 2M-8-48 -Pa.ds 100

WATER ANALYSIS

---~~p.-~~-~~---·---Factory

_________

Ap;r.t;:i. __

~3.~

__

_i.951

________________________

19 _________

_

Kind of Water:

W

ater used to

wash

white sugar

Average ~ample

for the 1950-51

Campaign

Source of Water:

Drips

from Steam Chest of 3rd effect of north evaporators

Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulfuric Acid SO,

Carbonic Acid

co.

Phosphoric Acid PO,

COPIES TO

General Chemist Asst_ General Supt. District Engineer

pH

Parts Per Million

Silica Si02

Sodium Carbonate Na2COs

Sodium Phosphate NasPO,

Magnesium Chloride MgCI.

Magnesium Phosphate Mgs(PO,).

Calcium Carbonate CaCOa

Calcium Phosphate Cas(PO,).

Ferrous Carbonate FeCOs

(9)

Form 443-2M-8-48- Pads 100

WATER ANALYSIS

.

..

.

....

..

~.J}~

.

~&~

...

.

..

.

...

.

....

.

Factory ...

~.P.r

.

:P~

.. -

~.3

.

, ..

.

l9.5.l

...

.

...

19 ... .

Kind of Water:

Boiler Feed

A

verage Sample for Campaign 1950-51

Source of Water:

- -

---ANALYSIS Silica SiO, Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulfuric Acid SO,

Carbonic Acid COs

Phosphoric Acid PO,

Drips from 2nd, 3rd, 4t

h

,

&

5th effects o

f

evaporators

Drips from pans after flashing to exhaust. All live

steam traps

HYPOTHETICAL COMBINATIONS Parts Per Million

Silica SiO,

Sodium Sulfate Na2SO,

Sodium Carbonate Na2COs

Sodium Phosphate NaaPO,

Ferrous Phosphate Fe,(PO,),

37.0

9.3

COPIES TO

General Chemist Asst. General Supt. District Engineer Superintendent Laboratory

pH

-7-Parts Per Million

37.0

(10)

Form 443 -2M- 8-48- Pads 100

...

.

...

~J.J!~g.~ ..

...

Factory Kind of Water: Description of Sample: Source of Water: ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulfuric Acid SO,

Carbonic Acid

co.

Phosphoric Acid PO,

WATER ANALYSIS

..

.

..

.

..

April

..

23 ,

..

.

1951

...

19 .

.

..

.

...

.

Water

in Boilers

Average Sample for Campaign

1950-51

Added to Boilers: Caustic Soda

Di Sod.Phosphate

Sodium. Sulphite

Alkalinity

Hardness

P0

4 Pounds

For Camp,

2400

900

300 Per

Day

27.7 llo3

3.5

Parts Per Million

9.0

Silica SiO,

3.5 trace

Sodium Sulfate Na2SO,

1.1

Sodium Carbonate Na,CO,

503.7

17.6

Magnesium Chloride MgCb

14404

525.7

Magnesium Carbonate MgCO,

65.0

Magnesium Phosphate Mg,(PO,).

Calcium Carbonate CaCO,

Calcium Phosphate Ca,(PO,).

Ferrous Carbonate FeCO,

Ferrous Phosphate Fe,(PO,),

E!li.

19

4

65 9o0

29.0

213.5

928.7

78.3

4.0

7.5 1270.0

759.0 1270.0

759.0 2029.0

_{TOTAL DISSOLVED SOLIDS AT 105° C}

2029.0

COPIES TO

General Chemist Asst. General Supt, District Engineer