Analysis of water for campaign 1945-1946 Billings factory

(1)

AJITALYSIS

OF

WATERS

FOR CAMPAIGN

1945-1946

BILLINGS FACTORY

THE GREA.T

W

ESTEill~ SUGAR COM

P

ANY

cc-

G

eneral Chemist

~

/

As

st.

Gen

.

Su:pt.

D

istrict

E

ngineer

Superintendent

Laboratory

(j . . . ~ - - •(

Chemist

(2)

INDEX:

KIND

OF

W

ATER

PAGE

M

ain

Tank

1 City

2

Battery

Supply

3

Press

,

iash

4

Centrifugal

W

ash

5

Cold

Saccharate

H

ash

6

Boiler Feed

7

(3)

Form 443-3M- 8-40-Pads 100

WATER ANALYSIS

···-

--~;l,J__:u:n.w

....

_______________

__________

Factory

...

-...

~~~

~

-

.

?.~

, ...

.:!-.

~1

~

....

...

.

19 4 ....

.

Kind of Water: Description of Sample: Source of Water: ANALYSIS Silica SiO, Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulfuric Acid

so.

Carbonic Acid

co

,

Phosphoric Acid PO,

Organic and Volatile (by difference)

Tank

Wa

ter

Average Sample for

the

1945-46 Campaign

Yellowstone River

Intake

one

mile south of Factory

Parts Per 100.000

2 .

02 .

18

4 .

00

1.46

3 .00

.

82

8 .17

7.92

27 .

57 .01

HYPOTHETICAL COMBINATIONS Silica Sodium Chloride Sodium Sulfate Sodium Carbonate SiO, NaCl Na.SO, Na.CO, Sodium Phosphate Na:iPO, Magnesium Chloride MgCl, Magnesium Sulfate MgSO,

Magnesium Carbonate MgCO,

Magnesium Phosphate MgJ(PO,h

Calcium Sulfate CaSO, Calcium Carbonate CaCO,

Calcium Phosphate Ferrous Carbonate Ferrous Phosphate

Ca,(PO,),

FeCO,. Fc,(PO,),

TOTAL SOLIDS AT 105° C

₂₇

_.58

COPIES TO General Supt. General Chemist Asst. General Supt. District Engineer Superintendent Laboratory

-1-Parts Per 100,000

2.02

1.35

7 .

63

3.77

2 .

43

10.00 .37

27 .

57

OJ

2

7.

58

Chief Chemist.

(4)

Form 443-SM-8-40•-Pads 100

WATER ANALYSIS

...

~~!~.

~.~~~····--··--··-·

-Factory

----·---~:1_f;l._Y. __

~l

._.J~1_9 _____

___

_

________

194 _____

_

Kind of Water: Description of Sample: Source of Water: ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulfuric Acid

so.

Carbonic Acid

co

,

Phosphoric Acid PO,

City

W

ater

A

ve

r

a

g

e

sample for the

1

9 45-46

Cama

p

ai

g

n

R

iver water

treated

and

filtered thru

0ity Water Plant

Parts Per 100.000

1.46 .17

4.29

1.46

3.26 .

82

8.50

8.45

28 .

41 .

87

HYPOTHETICAL COMBINATIONS Silica Si0,

Sodium Chloride NaCl Sodium Sulfate Na,SO, Sodium Carbonate Na,CO, Sodium Phosphate Na"PO, Magnesium Chloride MgCl2 Magnesium Sulfate MgSO, Magnesium Carbonate MgCO, Magnesium Phosphate Mg,(PO,), Calcium Sulfate CaSO, Calcium Carbonate CaCO, Calcium Phosphate Ca,(PO,), Ferrous Carbonate

Ferrous Phosphate

FeCOa Fe,(PO,),

29 .

28

COPIES TO General Supt. General Chemist Asst. General Supt. District Engineer Superintendent Laboratory

-2-Parts Per 100,000

1.46

1.35

8.43

3.51

2 .

60

10.71 .35

28.41 ,

8?

29.28

Chief Chemist.

(5)

Form 443-2M-7-43-,.Pads 100

WATER ANALYSIS

...

~iJJJ~&~

...

Factory

.

...

.

..

Ma

y.

2l.,.

..

l946

...

194 ..

...

.

· Kind of Water: Description of Sample: Source of Water: ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulfuric Acid S0₄ Carbonic Acid C03 Phosphoric Acid _P04

Battery Supply

Average Sample for

the

1945-46

Campaign

All

drips from

hot

condensors of evaporators,

drips

from

Vapor

Pan

,

overflow from press wash

HYPOTHETICAL COMBINATIONS Parts Per 100,000

1.20 .08

3.02

1.15

1.38 .

56

5 .

91

5 .

10

18.40

2 44 . Silica Si0₂

Sodium Chloride NaCl

Sodium Sulfate Na₂_S04

Sodium Carbonate Na2C03

Sodium Phos,phate Na₃_{P0 4}

Magnesium Chloride MgCl₂

Magnesium Sulfate _MgS04

Magnesium Carbonate MgC03

Magnesium Phosphate Mg3(P04)2

Calcium Sulfate CaS04

Calcium Carbonate _CaC03

Calcium Phosphate _Ca3(P04)₂

Ferrous Carbonate _FeC03

Ferrous Phosphate Fe₃_(P04)₂

Parts Per 100,000

1.20 .92

3.15 4o73

.

69

7.54 .

17

18 .

40

2 ,4,4,

_20.84

₂₀

_.

₈₄

COPIES TO

General Chemist Asst. General Supt. District Engineer Superintendent Laboratory

.. . .. . Chief Chemlat.

(6)

-3-Form 44S-2M-7-43---;-Pads 100

WATER ANALYSIS

....

.

...

..

.

...

~JJ.J.:i:ggf?.

....

...

Factory

...

.

May

.

21 .,.

.

. 1946 .

.

..

...

194 ...

.

Kind of Water: Description of Sample: Source of Water: Silica Iron Calcium Magnesium Sodium Chlorine Sulfuric Acid Carbonic Acid Phosphoric Acid Si02 Fe Ca Mg Na Cl S04 003 P0₄ ANALYSIS

Press

Wash

Average

sample for the 1945-46 CamJlpign

Condensed waters from all 1st effect Eavaporators

,

Battery

0alorisators, all heaters and overflow from Boiler .

.i:!'eed

.

Possible to send

Battery Supply to Press

11

_ash

_,

_and

_drips

from all evaporators, blow up traps, and offive heating

system

Parts Per 100,000 HYPOTHETICAL COMBINATIONS Silica Sodium Chloride Sodium Sulfate Sodium Carbonate Sodium Phos,phate Magnesium Chloride Magnesium Sulfate Magnesium Carbonate Magnesium Phosphate Calcium Sulfate Calcium Carbonate Calcium Phosphate Ferrous Carbonate Ferrous Phosphate Si02 NaCl Na2S04 Na₂C0₃ Na3P04 MgC1₂ MgS04 MgC03 Mg3(P04)2 CaS0₄ CaC03 Ca₃(P04 ) 2 FeC03 Fe3(P04 ) 2

Parts Per 100,000

3.6

3 .

6

COPIES TO

Cblet Chemist.

(7)

-4-Form 443- 2M-7-43-;Pads 100

WATER ANALYSIS

_

__

__________________

Bill

in& s

_____

_

_________

Factory

___

____

_

____

1.,:..a

y

_

21 ,

_

__

1946

_____

_

______

_

______

194 _

__

_

Kind of Water: Description of Sample: Source of Water: Silica Iron Calcium Magnesium Sodium Chlorine Sulfuric Acid Carbonic Acid Phosphoric Acid ANALYSIS Si02 Fe Ca Mg Na Cl S0₄ 003 P0₄

Water

used

tb

wash

white

sugar

Average sample for the

campaign

1945

-46

.urips

~ro

m

the steam

e

hest of the

3rd

effect

of the north

evaporators

Parts Per 100,000 HYPOTHETICAL COMBINATIONS Silica Sodium Chloride Sodium Sulfate Sodium Carbonate Sodium Phosphate Magnesium Chloride Magnesium Sulfate Magnesium Carbonate Magnesium Phosphate Calcium Sulfate Calcium Carbonate Calcium Phosphate Ferrous Carbonate Ferrous Phosphate Si0₂ NaCl Na2S04 Na2C08 Na₃P0₄ MgC1₂ MgS04 MgC03 Mg3(P04)2 CaS04 CaC03 Ca₃(P0_{4 )}₂ FeC03 Fe₃(P04) 2

2 .

4

COPIES TO

General Chemist Asst. General Supt, District Engineer Superintendent Laboratory

-5-Parts Per 100,000 ?

.

4

Chief Chemist.

(8)

Form 448-2M-7-43-;-Pads 100

WATER ANALYSIS

···-·.oill

in$s ____

·

--·--·--·-·--····Factory

···-···

Iay

__

21,

_

1946

...

lS,i ..

.

.. .

Kind of Water: Description of Sample:

Cold baccharate 0ake fosh ~fajier

Composite sample for the

last ten

days of the 1945-46

Camapaign

.

(City water

used the 1st 74

days)

Source of Water:

_lat

_{er fro}

_m

_{well so}

_ut

_h

_of

_{and adjac}

_ent

_{to limerock hopper+ press wash to temper.}

1946

Total Solids of

1ie

ll I

ater

Silica Iron Calcium Magnesium Sodium Chlorine Sulfuric Acid Carbonic Acid Phosphoric Acid Si02 Fe Ca Mg Na Cl S04 C0₃ P04 ANALYSIS

COPIES TO

General Chemist Asst. General Supt. District Engineer Superintendent Laboratory Parts Per 100,000

2.

56 .17

7.16

2 .

04

10 .74

1.84

23 .

41

13 .76

61.68

62

62 .

30 June 29

88 Aug

.

24 Oct

.

31 Dec

.

5 Final 10 days of

c.

-6-118

137

75

72

HYPOTHETICAL COMBINATIONS Silica Sodium Chloride Sodium Sulfate Sodium Carbonate

Sodium Phos,phate

Magnesium Chloride Magnesium Sulfate . Magnesium Carbonate Magnesium Phosphate Calcium Sulfate Calcium Carbonate Calcium Phosphate Ferrous Carbonate Ferrous Phosphate Si02 NaCl Na2S04 Na₂C0₃ Na₃P0₄ MgCl₂ MgS04 MgC03 Mg3(P04)2 CaS04 CaC0₃ Ca3(P04 ) 2 FeC03 Fe₃(P0₄)₂

TOTAL SOLIDS AT 105° C Parts Per 100,000

2.

56

3 .

03

29 .

50

4 .

34

4 .

02 17,88

.35

61.68 .62

62.30

Chief Chemist.

(9)

Form 443- 2M- 7-43-Pads 100

WATER ANALYSIS

Billings

F

...

.

...

.

..

.

..

...

..

.

..

.

...

.

..

.

...

.

..

. actory

...

.

...

1:ay

.

21 ,

__

l

946 ......................

194 ..

.

Kind of Water: Description of Sample: Source of Water: Silica Iron Calcium Magnesium Sodium Chlorine Sulfuric Acid Carbonic Acid Phosphoric Acid Si02 Fe Ca Mg Na Cl S04 C0₃ P04 ANALYSIS

l¥

ater

in

...,

oiler

.i..'eed Tank

Average

sample for the 1945-46

Campaign

Drips from

the

2nd,

3rd,

4th

&

5th bodies of

the evapo

rat

ors

.

All

live steam

traps

Parts Per 100,000 HYPOTHETICAL COMBINATIONS Silica Sodium Chloride Sodium Sulfate Sodium Carbonate Sodium Phos,phate Magnesium Chlorid~ Magnesium Sulfate Magnesium Carbonate Magnesium Phosphate Calcium Sulfate Calcium Carbonate Calcium Phosphate Ferrous Carbonate Ferrous Phosphate Si0₂ NaCl Na₂S0₄ Na2C03 Na₃P04 MgC1₂ MgS0₄ MgC0₃ Mg3(P04)2 CaS0₄ CaC0₃ Ca₈(P0₄)₂ FeC03 Fe₈(P04)2

Parts Per 100,000

_4.6

₄

_.

₆

COPIES TO

Chief Chemist.

(10)

-7-Form 448-2M-7-43--;-Pads 100

---

-

·

· ··

····

-

··-

Billings

.

..

...

.

...

.

....

Factory

Kind of Water: Description of Sample:

Added

to

Boilers:

Source of Water: ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulfuric Acid S04 Carbonic Acid C0₃ Phosphoric Acid P04

WATER ANALYSIS

Wa

ter in

Boilers

Average Sample

Caustic

Soda

Tri Sod

.

Phos

Sod

.

Sulphite

Soda Ash

Alkalinity

Hardness

P04

ppm

Parts Per 100,000

.

90

•

21 .15

.

23

31.85

1.99

5 .

58

34 .

23

5 .

80

80 .94

JS

-

06

... ~,Y. ..

21.,

.

.l94.6

...

..

.

....

.

..

.

...

194 .

...

. .

for the

1945-46

Campaign

For Camp

'

n

.

Per Day

4645

54 -

8 35?0

42 .

l

420

5 .

0

550

6 .

5 .

ooo

1,2

58

HYPOTHETICAL COMBINATIONS Silica Sodium Chloride Sodium Sulfate Sodium Carbonate Sodium Phosphate Magnesium Chloride Magnesium Sulfate Magnesium Carbonate Magnesium Phosphate Calcium Sulfate Calcium Carbonate Calcium Phosphate Ferrous Carbonate Ferrous Phosphate Si02 NaCl Na2S04 Na2C03 Na₃P0₄ MgC1₂ MgS0₄ MgC03 Mg3(P04)2 CaS04 CaC0₃ Ca3(P04)2 FeC0₃ Fe₃(P0_{4 )}₂