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Analysis of water samples for campaign 1925-1926 Billings factory

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(1)

ANALYSIS OF

ATER

SAMPLES

FOR

CAMPAIGN

1925-1926

BILLINGS FACTORY

THE GREAT WESTERN SUGAR

CO.MPANY

Copies to:

~

General

Chemist

A8st

.

Gen

.

Supt

.

Asst. Gen. Eng.

Superintendent

Laboratory

(2)

Yellowstone

River

l

City

2

Main Tank

Battery

Supply

(Single

System)

4

Hot

Press Wash

5

Evaporator

Condenser Tail Pipes

6

Pa.n

Condenser Tail Pipes

7

Boiler

Feed

Tank

8

Boiler

Feed

(Return

Direct)

9

Water

from Boilers

10

Surface

Water

ll

(3)

_

_

_ _ _

_

:B_i

_

·l_l_i

_

ng-=-s

_ _ _

__.

Factory

Ma.y

28th,

__ _ _

_I

9z

_

6

_

Kind of Water: Description of Sample: Source of Water: ANALYSIS Silica Si08 lroa Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulphuric Acid so.

Carbonic Acid co.

Organic and Volatile (by difference) TOT AL SOLIDS

COPIES TO

General Supt. General Chemist AIIISt.

Genl.

Supt. Asst. Chief Engineer Superintendent Traveling Chemist

Laboratory

Yellowstone RiTer

Water

Average

Sample for Campaign

Yellowstone River,

Intake one mile south of factory.

HYPOTHETICAL COMBINATIONS

Parta P .. 100,000

1.26

Silica Sio.

.14

Sodium Chloride NaCl

1.64

Sodium Sulphate Na2S04

1.70

Sodium Carbonate Na2C03

4.32

Magnesium Chloride

MgCI

1.22

Magnesium Sulphate MgS04

12.35

Magoesium c,..bonate MgC03

3.75

Calcium Chloride CaCl2

Calcium Sulphate easo,

Calcium Carbonate CaC03 Ferrous Carbonate FeC03

26.38

1.82

Organic and Volatile (by difference)

28.20

TOT AL SOLIDS

1

Parts Per 100,000

1.26

2.01

10.90

6.24

1.58

t

4.10

.29

26.38

l.82

28.20

Chief Chemist.

(4)

·THE GREAT WESTERN SUGAR COMPANY

_ _ _ _ _

B,M_,A,i ...

1,.1_.ingL_

____ _

_

__factory

- - - - -

May

28,

-~ --

_

192

_

6

_

Kiocl of Water: DescriptiQn of Sample: Source of Water: ANALYSIS Silica Si02 lroa Fe

Calcium

Ca Magn®um

Mg

Sodium Na Chlorine Cl Sulphuric Acid S04 Carbonic Acid C03

Organic and Volatile (by difference} TOT AL SOLIDS

COPIES TO General Supt. General Chemist A91St. Genl. Supt. A.st. Chief Engin-Superintendent Traveling Chemist Laboratory

City

Water

ATera.ge Sample for Campaign

Yellowstone

RiTer,

Filtered thru. City

Filtering Plant

HYPOTHETICAL COMl:HNATIONS

Parta P« l 00,000 Porta Per 100.000

1.06

Silica Si02

1.06

.23

Sodium Chloride NaCl

l.68

2.10

Sodium Sulphate Na2S04

7.41

1.35

Sodium Carbonate Na1C03

3.06

Magnesium Chloride MgCI

1.02

Magnesium Sulphate MgS04

6.71

10.37

Magnesium c,.bonate MgC03

3.39

Calcium Chloride CaCl2

Calcium Sulphate CaS04

Calcium Carbonate CaC08

5.24

Ferrous Carbonate FeC03

.48

22.58

22.58

.98

Organic and Volatile ( by difference)

.98

23.56

TOT AL SOLIDS

23.56

2

(5)

_ _ _ _ _ _

BU.,Li.1 ..

1...,icL!ngf",..<la

,_

_ _ _

_factory

_ _

19~

-Kind of Water: DescriptiQn of Sample: Source of Water: ANALYSIS Silica Si02 lroa Fe Calcium Ca Magnelium Mg Sodium Na Chlorine Cl

Sulphuric Acid

so.

Carbonic Acid C03

Organic and Volatile (by difference) TOT AL SOLIDS

COPIES TO General Supt, General Chemist Asst. Genl. Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory

Main

Ta.nlc

Ayera.ge

Sample

for Campaign

Yellowstone

RiYer,

Possible to send city water to this tank

1Tain

source of supply for all factory operations

Parts p.., 100,000

1.42

.16

l.79

1.38

4.36

1.08

12.26

3.57

26.02

3.94

29.96

HYPOTHETICAL COMBINATIONS Silica Si02

Sodium Chloride NaCl

Sodium Sulphate Na2S04

Sodium Carbonate Na2C03

Magnesium Chloride MgCI

Magnesium Sulphate MgS04

Magnesium C.,,bonate MgC03

Calcium Chloride

eac1

2 Calcium Sulphate

easo.

Calcium Carbonate CaC08

F erroua Carbonate FeC03

Or11anic and Volatile (by difference)

TOT AL SOLIDS Parts Per I 00,000

ll.30

5.71

1.01

4.47

.33

26.02

3.94

29.96

Chief Chemi,1.

(6)

J3illings

Kind of Water: DescriptiQn of Sample: Source of Water: ANALYSIS Silica Si02 lroa Fe Calcium Ca Magn~ium Mg Sodium Na Chlorine Cl Sulphuric Acid S04 Carbonic Acid C03

Organic aad Volatile (by difference) TOT AL SOLIDS COPIES TO

General Supt. General Chemist A .. t. Genl. Supt. AssL Chief Engineer Superintendent Traveling Chemist Laboratory

THE GREAT WESTERN SUGAR COMPANY

_Factory

J3attery Supply, (Single System)

Average sample tor

Campaign

192

_

6

_

All waters

from upper condensers of

3

vaporators(Tail

?ipes)

Drip

waters

from Vapor pan,

Possible

to send water from main tank

Pam P« 100,000

l.76

.22

2.02

l.43

4

.1

4

1.12

ll.32

4

.35

26.34

5

.1

2

31.46

4

HYPOTHETICAL COMBINATIONS Silica Si02

Sodium Chloride NaCl

Sodium Sulphate Na2S04

Sodium Carbonate Na.C03

Magnesium Chloride MgCl

Magnesium Sulphate MgS04

Magnesium C..bonate MgC03

Calcium Chloride CaCI2

Calcium Sulphate

easo.

Calcium Carbonate CaC03

Ferrous Carbonate FeC03

Organic and Volatile l by difference)

TOT AL SOLIDS Parts Per 100.006

5.04

.46

26.34

5.12

(7)

Billings

Kind of Water: DescriptiGn of Sample: Source of Water: Silica lroa Cakium Magn,ruum Sodium Chlorine Sulphuric Acid Carbonic Acid Si02 Fe Ca Mg Na Cl C03 ANALYSIS

Organic and Volatile (by difference) TOT AL SOLIDS COPIES TO

Gen~al Supt. General Chemist A .. t. Genl. Supt. A•t. Chief Engineer Superintendent Traveling Chemist Laboratory

_Factory

Hot Press

W

ash

ATera.ge for Campaign

~

~l

28.

Candensed waters from 1st. Effe

~

t Evaporators,

Battery Calorisators, all heaters and overflow

B

oiler feed

Tank.

Possible to send Battery Supply

to Press Wash and drips from

all

eya.pora.tors,

carbonation and blow-up traps and office heating

system

. ___

192_

6

_

HYf;'OTHETICAL COMBINATIONS Part. P« 100,000

.36

.20

.44

.17

.51

.30

74

l.24

3.96

1.78

5.76

5

Silica Si02

Sodium Chloride NaCl

Sodium Sulphate Na2S04

Sodium Carbonate Na2C03

Magnesium Chloride MgCI

Magnesium Sulphate MgS04

Magnesium c..,bonate MgC03

Calcium Chloride CaCl2

Calcium Sulphate CaSO,

Calcium Carbonate CaC03

Ferrous Carbonate FeC03

Organic and Volatile (by difference)

TOT AL SOLIDS Part, Per 100,000

.38

.49

.99

.09

.52

1.10

.41

3.98

l,78

Chief Chemi,1.

(8)

Bi 11 i:ggs

Kind of Water: Description of Sample: Source of Water: ANALYSIS Silica Si02 lroe Fe Cakium Ca MagneMum Mg Sodium Na Chlorine Cl Sulphuric Acid S04 Carbonic Acid

co

.

Organic and Volatile. (by difference) TOT AL SOLIDS COPIES TO

General Supt. General Chemist A!St.

Genl.

Supt. Asst. Chief Engineer Superintendent Traveling Chemist Laboratory

THE GREAT WESTERN SUGAR COMPANY

_

.Factory

Condenser Tail Pipes of E'YB.po

r

ators

AYerage

sample for Campaign

V

J.a.in

W

ater Tank,

{

Ma.

in source of supply for all

F

actory operations)

HYPOTHETICAL COMBINATIONS

Parta Pe< 100,000

2.04

Silica Si02

.14

Sodium Chloride NaCl

2.08

Sodium Sulphate Na2S04

1.31

Sodium Carbonate Na2C03

5.20

Magnesium Chloride MgCI

1.12

Magnesium Sulphate MgS04

12.06

Magnesium C,.:bonate MgC03

4.79

Calcium Chloride CaCl2

Calcium Sulphate CaS04

Calcium Carbonate CaCO"

Ferrous Carbonate FeC03

28.74

l.lO

Organic and Volatile (by difference)

29.84

TOT AL SOLIDS

6

_

192_6__

Parts Per I 00,000

2.04

l.85

13.81

3.41

2.15

5.19

.29

28.74

1.10

29.84

Chief Chemist.

(9)

:Billings

Kiod of Water: Description of Sample: Source of Water: ANALYSIS Silica Si02 lroa Fe Cailcium Ca Magn~ium Mg Sodium Na Chlorine Cl Sulphuric Acid S04

Carbonic Acid

co.

Organic and Volatile (by difference) TOT AL SOLIDS COPIES TO

Genrral Supt. General Chemist A11St. Genl. Supt. AllBt. Chief Engineer Superintendent Traveling Chemiet Laboratory

Factory

Condenser Tail

Pipes

of Pans

Average

sample for Campaign

W.a.in Tank,

(

Main

source of

Supply

for all factory operations)

HYPOTHETICAL COMBINATIONS

Paro Per I 00.000

2.50

Silica Si02

.15

Sodium Chloride NaCl

2.39

Sodium Sulphate Na2S04

1.29

Sodium Carbonate Na2C03

4.01

Magnesium Chloride MgCl

1.02

Magnesium Sulphate MgS04

11.31

Magnesium C:\rbonate MgC03

4.22

Calcium Chloride CaC12

Calcium Sulphate

easo.

Calcium Carbonate CaC03

Ferrous Carbonate FeC03

26.90

1.40

Organic and Volatile ( by di ff ere nee)

28.30

TOT AL SOLIDS

7

192

_

6

_

Part, Per 100.000

2.50

1.68

10.35

5.40

.69

5.97

.31

26.90

laiO

28.30

Chief Chemist.

(10)

_

_

__

B

_

1.

_

· l

_

l

_

1._·

ng~l

_ _ _ _ _ _

f

actory

_

J92

_

6

_

Kind of Water: Description of Sample: Source of Water: ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodinm Na Chlorine Cl Sulphuric Acid S04 Carbouic Acid C03

Organic a11<l Volatile (by difference) TOTAL SOLIDS COPIES TO

General Snpt. General Chemist

Asst. Genl. Supt. Asst. Chief Enirineer

Sn perin tend en t

Traveling Chemist

Laboratory

Boiler

feed

Ta.nk

Average Sample

for Campaign

Drips from

2nd.,

3rd., 4th.,

and 5th.

Bodies

of the

Evaporators. Drips

from all live steam, all granulators

and all

heating

systems, 1st., 2nd., and 3rd. Condensers,

and

Blow-up Traps.

P

ossible to send drips from all heaters.

HYPOTHETICAL COMBINATIONS

Part, Per 1001000 Parts Per 100,000

.48

Silica Si02

.48

.05

Sodium Chloride NaCl

.68

.24

Sodium Sulphate Na2R04

.96

.12

Sodium Carbonate Na2C03

.58

Magnesium Chloride MgCI

.41

Magnesium Sulphate MgS04

.21

.82

Magnesium Carbonate MgC03

.27

.60

Calcinm Chloride CaCh Calcium Sulphate CaS04

Calcium Carbonate CaC03

.60

Ferrous Carbonate FeC03

.10

- - -

·

-3.30

3.30

.90

Organic and Volatile ( by difference)

.90

4.20

TOTAL SOLIDS

~.20

8

(11)

_,

- -

---'

::B=-=il=l=i=ng=s

_ _ _ _ _

f

actory

Ma.y--28

t- _ _

J

92.6

_.

Kind of Water:

Description of Sample:

Source of -water:

:Boiler

Feed

(Return

Direct)

Average Sample

for Campaign

·

All

c~ondensed

waters

from

pan coils except

from

Vapor

Pan.

Passed

direct

to

Boilers.

ANALYSIS HYPOTHETICAL COMBINATIONS

Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid S04 Carbonic Acid C03

Organic and Volatile (by difference)

TOTAL SOLIDS

COPIES TO General Supt. General Chemist Asst. Genl. i-:lupt. Asst. Chief Engineer

Rn perin ten dent

Traveling Chemist Laboratory Parts Per 100,000

.ao

.10

.59

.12

.72

.30

l.52

l.04

5.19

1-57

6.76

9

Silica Si02

Sodium Chloride NaCl

Sodium Sulphate Na2~04

Sodium Carbonate Na2C03

Magnesium Chloride MgCl

M::fgnesium Sulphate MgS04

Magnesium Carbonate MgC03

Calcium Chloride CaCh

Calcium .Sulphate CnS04

Calcium Carbonate CaC03

Ferrous Carbonate FeC03

Or~anic and Volatile (by difference)

TOTAL SOLIDS Parts Per 100.000

.ao

049

l.64

.51

.07

l.47

.21

5.19

6.76

Chief Chemist.

(12)

- -

- -

-

..

:B~i..i.l...i.l,a.i..ing~s----F

actory

. ~

Ma.Y

2a,

~ - -

l92_6_

Kind of Water: Description of Sample: Source of ,vater: ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulphuric Acid S04 Carbonic Acid C03

Organic and Volatile (by difference) TOTAL SOLIDS COPIES TO

General Snpt. General Chemist Asst. Genl. Supt. Asst. Chief Engineer 8nperintendent

Traveling Chemist

Laboratory

Boiler Water

Average

Sample for Campaign

Water in Boilers:- Contains

drips from pan coils and

Water

from

Boiler .

t

eed

Tank.

Also

contains

wa.ter

softeners.

HYPOTHETICAL CO MBIN A TIO NS Part, Per I 00,000

7.20

Silica Si02

.22

Sodium Chloride NaCl

.51

Sodium Sulphate Na2S04

.13

:',odium Carbonate Na2C03

37.31

Magnesium Chloride MgCI

1.73

Magnesium Sulphate MgS04

13.62

Magnesium Carbonate MgC03

40.02

Calcium Chloride CaCh Calcium Sulphate CaS04 Calcium Carbonate CaC03 Ferrous Carbonate FeC03

100.74

26.56

Organic and Volatile (by difference)

127.30

TOTAL SOLIDS

10

Parts Per I 00,000

7.20

2.85

20.14

68.37

.

45

1.27

.46

100. 74

26.56

127.30

Chief Chemist.

(13)

-

- - - - -

~B~i=l=l=i=ng""-'-'s~

_ _ _

f actory

~y

~th • .,

_ _

_

)926

__

Kind of Water: Description of Sample: Source of Water: ANALYSIS Silica Si02 Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl Sulplrnric Acid

804

Carbonic Acid C03

Organic and Volatile (by difference) TOTAL SOLIDS

COPIES TO

General Snpt. General Chemist Asst. GPnl. Supt, Asst. Chief Engineer Sn perin tend en t

Traveling Chemist

Laboratory

t

Surface

Water.

Sample ta.ken during

February

1926.

Surface ~ater draining into small well that

was

sunk

to enable foot valves of main water

pumps to be lowered.

Used to flume

a.shes

during campaign.

Used as

Boiler

Feed during intercampa.iB'Il•

(Cut scale on

Boiler

tubes)

Parts Per I 00,000

3.48

.70

11.91

11.47

56.59

a.so

155.14

16.32

264.41

17.99

282.40

11

HYPOTHETICAL CO :\!BIN A TIO NS

Silica Si02

Sodium Chloride NaCl

Sodium Sulphate Na2R04

Sodium Carbonate Na2C03

Magnesium Chloride MgCl

Magnesium Sulphate MgS04

Magnesium Carbonate MgC03

Calcium Chloride CaCh

Calcium Sulphate CaS04

Calcium Carbonate CaC03

Ferrous Carbonate FeC03

Organic and Volatile (by difference) TOTAL SOLIDS

- - - -

-Parb Per 100,000

3.48

14.51

157.14

56.72

264.41

17.99

282.40

Chief Chemist,

References

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