Analysis of water samples for the campaign 1931-32 Billings factory

(1)

' /

Hnl.YSIS

OF

W

.. \.'

l1ERS FCR

C,\.HPli.IC·N

1931-1932

BILLIUGS

Fl..C'.I'ORY

1

_.I.1:-:E

_GRE.A'I1 _WES11_Z?.}T _SUGAR

_COMl?ANY

Copies to;

General

Chemist..--,--sst.Gen.

E!lg

.

?:rotne.ge

r

Superintendent

Laboratory

(2)

INDEX

KIN1 OF WATER

PAG~

Yellowstdme River

l

City

2

Battery Zupply

3

Press

\Jash

4

Boiler Feed

5

(3)

_____________

E

il

1 ings _________________________

Factory

Kind of Water: Description of Sample: Source of Water: ANALYSIS Silica SiO, Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulphuric Acid

so,

Carbonic Acid

co.

Organic and Volatile (by difference) TOTAL SOLIDS COPIES TO

General Supt. General Chemist Asst. General Supt. Asst. Chief Engineer Superintendent Laboratory

WATER

ANALYSIS

______ .f.~Pr~1-':'

.

r:1.

.

?~.1. _____

__

_____________

_

____

1932

River Water

,,ere.ge

Sam11le

for Campaiftn

Yellowstone P

iver

Intake one

mile

south of I<'actory

i..lke.linity

,

due

~o

:!yd.rate.

s

---..---

0.0 .

H/28 H2S04

Parts P e ~ O O

2 .

20 .17

4.86

1 .75

4.41

1.10

13 .

79

8 .00

36.28 .

42

36 .70

l

HYPOTHETICAL COMBINATIONS Silica SiO,

Sodium Chloride NaCl

Sodium Sulphate Na,SO, Sodium Carbonate Na,CO,

Magnesium Chloride MgCl

Magnesium Sulphate MgSO,

Magnesium Carbonate MgCO, Calcium Chloride CaCl, Calcium Sulphate CaSO, Calcium Carbonate CaCO, Ferrous Carbonate FeCO.

Organic and Volatile (by difference) TOTAL SOLIDS Parts Per 100,000

2.20

1.81

11.43

7 .

59 .76

12.14 .35

36 .

28 d£

36 .

70

Chief Chemist.

(4)

____________________ }3

ill

ings

_________

____

_____

Factory

Kind of Water: Description of Sample: Source of Water: ANALYSIS Silica SiO, Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulphuric Acid

so.

Carbonic Acid

co,

General Supt. General Chemist Asst. General Supt. Asst. Chief Engineer Superintendent

WATER ANALYSIS

---

---~-~-~!~--~~X ...

?.~_,_ ______________

193

2 City Nater

verace Sample for Campaign

Yellowstone

Fi

ver

Water filtered thru

City Filtering :Plant

.ilkalini:ri

due to

Fydrates

---

0 .0

N/28

H

2 s

~

4

Parts Per 100,000 ~

2 .

14 .11

4.89 ··

1.

72

4 .

15 ·,l.10

13.41

7.79

35.31

1.09

36.40

HYPOTHETICAL COMBINATIONS Silica SiO,

Sodium Sulphate Na2SO. Sodium Carbonate Na2CO,

Magnesium Chloride MgCl Magnesium Sulphate MgSO, Magnesium Carbonate MgCO,

Calcium Chloride CaCl2

Calcium Sulphate CaSO,

Calcium Carbonate CaCO,

Ferrous Carbonate FeCO,

Organic and Volatile (by difference) TOTAL SOLIDS Parts Per 100,000

2.1

L.81

10.62

7.81 .49<

12. 21

~23

35.31

1.09 36,40

(5)

__________ Billi~g_i;i _______________________

__

____

Factory

Sulphuric Acid

so.

Carbonic Acid

co

.

General Supt_ General Chemist Asst. General Supt. Asst. Chief Engineer Superintendent Laboratory

WATER ANALYSIS

______________ f

_

~_Qfl~~-:r.y __ ~

_

!;)

_~

-

---

-

---

193

2 Battery Supply

Averase Sample for Campaign

All waters from the k~per condensors of

Evaporetors,

Drips from Ve.po

r

Pan

,

Overflow

from Press i,ash

,,1.lkalinity

d~e

to

Hydrates

----

---

0 .

0 N/28

H2S04

HYPOTHETICAL COMBINATIONS

Parts P~OOO Parts Per 100,000

2 .

22 .

31

3 .

93

1.52

4. 37

1 .

34

11.11 7,60

32 .

40 .32

32 .

72

3 Silica Si02

Sodium Sulphate Na2SO, Sodium Carbonate Na2COa

Magnesium Chloride MgCl Magnesium Sulphate MgSO, Magnesium Carbonate MgCOs

Calcium Chloride CaCl,

Calcium Sulphate CaSO.

Calcium Carbonate CaCO.

Organic and Volatile (by difference) TOTAL SOLIDS

2 .

22

2.21

10 .

81

4 ,

76

1. ~4

9 .

82

•

64

32 .

4.-0

.32

32 .

72

Chief Chemist.

(6)

WATER ANALYSIS

···---~j,.J.Jt~~g_fl ...

Factory

-

---

· -·--···-Jf.eJu:~~

.

:r.Y.. ..

?

.

!2

-.

..

.

...

.

193

2

Sulphuric Acid

so.

Carbonic Acid

co

.

Organic and Volatile (by diffe1·ence) TOTAL SOLIDS COPIES TO

General Supt. General Chemist Asst. General Supt. Asst. Chief Engineer Superintendent

Pre

ss

''ash

;~vere.ge Sample for Campaign

Condensed waters from

all 1st

.

EU·ect l:!;vRpora.tors

,

Battery

Calorisators

,

all heaters

e.na. overflow f

r

o'.11 Boiler

l!

'

eed

1

i1

_ank

_.

ossible to send Batter~, sup~,

ly to !'r

ess \1ash,

and

nr:i.ps fro,n all

evaporators, car"bo

-

.a

t

i

ol!l

im

d

Blow-up tr:::.ps,

a.

nd

office heatine

sy

stem.

Alkalinity

due

to :'.:Iydrates ---

o.o

1rj2e

H2~04

Parts Per 100,000

.

30 .04

.

16 .

12 .

60

•

35

1.09 .

38

3 .

04

1.80

4 .

84

HYPOTHETICAL COMBINATIONS Silica SiO, Sodium Chloride NaCl Sodium Sulphate Na,SO,

Sodium Carbonate Na,COo

Magnesium Chloride MgCl

Magnesium Carbonate MgCO,

Calcium Chloride CaCl2

Calcium Sulphate CaSO, Calcium Carbonate CaCOo

Ferrous Carbonate FeCOa

Organic and Volatile (by difference)

TOTAL SOLIDS Parts Per 100,000

.

30

•

58

1 ,

14 .

':i:O

.

14

• .,,o

.

08

3 .

04

1.

80

4.8':

(7)

WATER ANALYSIS

_

_______

____

__

B.illings __________________

Factory

_______

:teJ:n::~ne..r_y __

?,_Q_, _________________________

193

2

Kind of Water:

Boiler

Feed

Description of Sample:

1..verage 5&.mple for Cempai&n

Source of Water: ANALYSIS Silica SiO, Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulphuric Acid so, Carbonic Acid co.

General Supt. General Chemist Asst. General Supt. Asst. Chief Engineer Superintendent Laboratory

Drips from 2ncL,

3rd.

.,

4tr.,

•.nG.

5tb.~od.ies of

Flva.por9.tors,

Dri:ls fro.n

e

.

11 L.ve steam

,

all

<.£ranula.tors,

anc.

all

heating

sy ste!".ls, 1st.

,

?.na

.• ,

s.nd 3r6..

r;onc.eneor

s s.r~d blow-up

tra.:p

s.

Possiole to senc...

a.rips

from

all beaters.

~

J.kalinity

due

t(?

H7drates ---

-

--

o.o

ml.

E/28

R

₂

so

₄

HYPOTHETICAL COMBINATIONS

Parts Per 100,000 Parts Per 100,000

.12

.02

.23

.15

.21

.15

.70

.

43

2.01

• bb

2.66

5 Silica Si02

Sodium Chloride NaCl Sodium Sulphate Na,SO, Sodium Carbonate Na,COa

Magnesium Chloride MgCl Magnesium Sulphate MgSO, Magnesium Carbonate MgCOa Calcium Chloride CaCl, Calcium Sulphate CaSO, Calcium Carbonate caco.

Organic and Volatile (by difference) TOTAL SOLIDS

.

12 .25

.34

• 59

, 10

.

57 .04

2 .01

~ b5 2.06 Chief Chemist.

(8)

WATER

ANALYSIS

___________________ :Sill

ings __________

_

________

Factory

__

_

__

___

F.-?;Y.

;?_E?_L_ ___________________

l93

2

Kind of Water:

Boiler Water.

Description of Sample:

_{Average Sample from Boilers for the 1931-32 Campaign.}

Source of Water:

_{From Boiler}

_Feed

_{Tank and City}

_{water snpply.}

For

Ca.mpe.ign

:Per

Day

Pounds Soda

.Ash

added to

:Eoilers

700

6.9 Pounds

Caustic

Soda added to

Boilers

250

295 Alke

.

linity

due to

H

ydrates

---

o.o

_{ml. N/28 R2}

so

₄

ANALYSIS Silica SiO, Iron Fe Calcium Ca Magnesium Mg Sodium Na Chlorine Cl

Sulphuric Acid

so,

Carbonic Acid

co.

General Supt. General Chemist Asst. General Supt. Asst. Chief Engineer Superintendent Parts Per 100,000

31165

g49

2.75 .19

30 .. 17

1.65 12,.72

35.14 86~ 76

2 7 ~

114 ..

30

HYPOTHETICAL COMBINATIONS

I

Silica Si02

I

Sodium Sulphate Na2SO,

Sodium Carbonate Na2COa

Magnesium Chloride MgCI

Magnesium Carbonate MgCOa

Calcium Chloride CaCl,

Calcium Sulphate CaSO,

Calcium Carbonate CaCO,

Ferrous Carbonate FeCOa

Organic and Volatile (by difference)

TOTAL SOLIDS Parts Per 100,000

3,65

2,72

18.81

53.03 .66

6.87

1.02

86.76

27.54 114. 30